Unlock instant, AI-driven research and patent intelligence for your innovation.

Preparation method of high-activity titanium-based tantalum coating with micro-nano multilevel structure

A high-activity, tantalum coating technology, applied in coating, metal material coating technology, medical science and other directions, to achieve the effect of improving biological activity and improving protein adsorption capacity

Pending Publication Date: 2022-01-28
广东省华源康泰生物科技有限责任公司
View PDF2 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Currently, such structures cannot be constructed quickly and efficiently by conventional chemical or electrochemical methods

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Preparation method of high-activity titanium-based tantalum coating with micro-nano multilevel structure
  • Preparation method of high-activity titanium-based tantalum coating with micro-nano multilevel structure
  • Preparation method of high-activity titanium-based tantalum coating with micro-nano multilevel structure

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] This embodiment provides a method for preparing a highly active titanium-based tantalum coating with a micro-nano multi-level structure, comprising the following steps:

[0031] 1) Select tantalum powder (w(Ta)≥99.5%) with a particle size of 45-105μm as the raw material for spraying, and the powder appearance is as follows figure 1 As shown, the powder is spherical and has good fluidity; the powder is dried at 60°C for 30 minutes, and cooled for later use.

[0032] 2), using Al 2 o 3 The powder is subjected to sandblasting pretreatment on the titanium-based material. The sandblasting pressure is 0.8MPa, and then ultrasonically cleaned with acetone, ethanol and deionized water for 15 minutes, dried at 60°C for 30 minutes, and cooled for later use;

[0033] 3), using atmospheric plasma spraying technology, spray the tantalum powder prepared in step 1) onto the surface of the titanium-based material after sandblasting in step 2), and prepare a tantalum coating with a thi...

Embodiment 2

[0040] This embodiment provides a method for preparing a highly active titanium-based tantalum coating with a micro-nano multi-level structure, comprising the following steps:

[0041] (1) Select tantalum powder (w(Ta)≥99.5%) with a particle size of 45-105μm as the raw material for spraying, and the powder appearance is as follows figure 1 As shown, the powder is spherical and has good fluidity. Dry the powder at 60°C for 30 minutes, and cool it for later use.

[0042] (2) Using Al 2 o 3 The powder is subjected to sandblasting pretreatment on the titanium-based material. The sandblasting pressure is 0.8MPa, and then ultrasonically cleaned with acetone, ethanol and deionized water for 15 minutes, dried at 60°C for 30 minutes, and cooled for later use;

[0043] (3) using atmospheric plasma spraying technology, spraying the tantalum powder prepared in step (1) to the surface of the titanium-based material after sandblasting in step (2), and preparing a tantalum coating with a ...

Embodiment 3

[0049] This embodiment provides a method for preparing a highly active titanium-based tantalum coating with a micro-nano multi-level structure, comprising the following steps:

[0050] (1) Select tantalum powder (w(Ta)≥99.5%) with a particle size of 45-105μm as the raw material for spraying, and the powder appearance is as follows figure 1 As shown, the powder is spherical and has good fluidity. Dry the powder at 60°C for 30 minutes, and cool it for later use.

[0051] (2) Using Al 2 o 3 The powder is subjected to sandblasting pretreatment on the titanium-based material. The sandblasting pressure is 0.8MPa, and then ultrasonically cleaned with acetone, ethanol and deionized water for 15 minutes, dried at 60°C for 30 minutes, and cooled for later use;

[0052] (3) using atmospheric plasma spraying technology, spraying the tantalum powder prepared in step (1) onto the surface of the titanium-based material after sandblasting in step (2), and preparing a tantalum coating with a...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
thicknessaaaaaaaaaa
thicknessaaaaaaaaaa
thicknessaaaaaaaaaa
Login to View More

Abstract

The invention provides a preparation method of a high-activity titanium-based tantalum coating with a micro-nano multilevel structure. The method comprises the following steps that S1) sand blasting treatment is carried out on the surface of titanium-based metal, and the high-activity titanium-based tantalum coating is prepared on the surface of the titanium-based metal by taking tantalum powder with high biological activity as a raw material and using a plasma spraying technology; and S2) the surface of the high-activity titanium-based tantalum coating material is subjected to laser irradiation treatment, at the moment, the surface of the titanium-based tantalum coating absorbs laser energy to be fused and cooled in the air atmosphere, a groove and a fused material accumulation area are generated, meanwhile, steam and plasma expansion plumes are generated to escape in the air, and quickly cooling is carried out to form nanoscale particles which are stacked on the surface of the coating, and finally a micro-nano multi-stage structure consisting of grooves, molten material stacking, quick cooling particle stacking and the like is formed. According to the obtained high-activity titanium-based tantalum coating with the micro-nano multilevel structure, the micro-nano multilevel structure of bone tissue is simulated while an active material is introduced, and the biological activity is remarkably improved.

Description

technical field [0001] The invention relates to the technical field of biomedical materials, in particular to a method for preparing a highly active titanium-based tantalum coating with a micro-nano multi-level structure. Background technique [0002] Due to its excellent mechanical properties and easy processing, titanium-based metals have become one of the most clinically used biomaterials in the field of orthopedic implants. [0003] However, the surface of titanium-based metals is biologically inert, and it is difficult to directly chemically bond with bone tissue. The bone formation rate after implantation in the body is slow, and the clinical application effect needs to be improved. Therefore, surface modification of titanium-based metals is an important way to solve the above problems. [0004] At present, the idea of ​​surface modification of titanium-based metals is to introduce new materials with high bioactivity to make coatings; on the other hand, it is to imita...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C23C4/134C23C4/18A61L27/30C23C4/08
CPCC23C4/134C23C4/08C23C4/18A61L27/306
Inventor 张芳郑裕民
Owner 广东省华源康泰生物科技有限责任公司