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Gradient material and preparation method thereof

A gradient material and manufacturing method technology, applied in the direction of additive manufacturing, additive processing, metal processing equipment, etc., can solve the composition, structure and stress discontinuity, ferritic martensitic steel and austenitic stainless steel composition and microscopic Problems such as large tissue differences and easy failure can be achieved to improve service safety, uniform hardness and tissue transition, and increase service life.

Pending Publication Date: 2022-02-01
CHINA INSTITUTE OF ATOMIC ENERGY +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the high solubility of nickel in lead or lead-bismuth, this welded dissimilar structure is not suitable for nuclear test devices and fast neutron reactors cooled by lead or lead-bismuth
In addition, the traditional welding method forms a single transition zone at the welded joint of dissimilar steels, while ferritic martensitic steel and austenitic stainless steel have large differences in composition and microstructure. In this single transition zone, there are large composition, Tissue and stress discontinuities
Studies have shown that this discontinuity causes welded joints of dissimilar steels to fail more easily than joints of the same steel, which is directly related to the reliability and safety of the device
[0003] Therefore, there is a need to develop new joining methods of dissimilar alloys to solve the problem that traditionally welded components are not suitable for the requirements of lead or lead-bismuth cooled reactor systems

Method used

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  • Gradient material and preparation method thereof
  • Gradient material and preparation method thereof
  • Gradient material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0080] Embodiment 1 prepares T91 / 316H type gradient material (gradient 10%)

[0081] Preparation of T91 steel powder and 316H stainless steel powder

[0082] Prepare the corresponding 316H and T91 homogeneous alloy ingots, and gas atomize the homogeneous alloy ingots; then perform drying treatment and deoxidation treatment so that the oxygen content is ≤ 10ppm, and perform air classification and powder batching to obtain 316H pre-alloyed powder with a purity ≥ 99.5% and a particle size range of 50-153 μm, and T91 pre-alloyed powder with a purity ≥ 99.5% and a particle size range of 50-153 μm.

[0083] Laser Additive Manufacturing Gradient Materials

[0084] Evacuate the air in the print chamber and fill it with argon. Wipe the surface of the 304 stainless steel substrate with alcohol, dry it, place it on the platform of the CNC machine tool and preheat it to 80°C.

[0085] First, 20 layers of T91 steel were printed on the substrate with the above-mentioned pre-alloyed powde...

Embodiment 2

[0098] Embodiment 2 prepares T91 / 316H type gradient material (gradient 20%)

[0099] Preparation of T91 steel powder and 316H stainless steel powder

[0100] Prepare the corresponding 316H and T91 homogeneous alloy ingots, and gas atomize the homogeneous alloy ingots; then perform drying treatment and deoxidation treatment so that the oxygen content is ≤ 10ppm, and perform air classification and powder batching to obtain 316H pre-alloyed powder with a purity ≥ 99.5% and a particle size range of 50-153 μm, and T91 pre-alloyed powder with a purity ≥ 99.5% and a particle size range of 50-153 μm.

[0101] Laser Additive Manufacturing Gradient Materials

[0102] Evacuate the air in the print chamber and fill it with argon. Wipe the surface of the 304 stainless steel substrate with alcohol, dry it, place it on the platform of the CNC machine tool and preheat it to 80°C.

[0103] First, 40 layers of T91 steel were printed on the substrate with the above-mentioned pre-alloyed powde...

Embodiment 3

[0112] Embodiment 3 prepares T91 / 316H type gradient material (gradient 5%)

[0113] Preparation of T91 steel powder and 316H stainless steel powder

[0114] Prepare the corresponding 316H and T91 homogeneous alloy ingots, and gas atomize the homogeneous alloy ingots; then perform drying treatment and deoxidation treatment so that the oxygen content is ≤ 10ppm, and perform air classification and powder batching to obtain 316H pre-alloyed powder with a purity ≥ 99.5% and a particle size range of 50-153 μm, and T91 pre-alloyed powder with a purity ≥ 99.5% and a particle size range of 50-153 μm.

[0115] Laser Additive Manufacturing Gradient Materials

[0116] Evacuate the air in the print chamber and fill it with argon. Wipe the surface of the 304 stainless steel substrate with alcohol, dry it, place it on the platform of the CNC machine tool and preheat it to 80°C.

[0117] First, 40 layers of T91 steel were printed on the substrate with the above-mentioned pre-alloyed powder...

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Abstract

The invention discloses an alloy material, and particularly relates to a gradient material for connecting dissimilar steel, such as T91 steel and 316H stainless steel. The gradient material is provided with a T91 steel layer, a transition layer and a 316H stainless steel layer which are sequentially stacked, in the transition layer, the sum of the weight percentage of T91 steel and the weight percentage of 316H stainless steel is 100%, and the weight percentage of the T91 steel is decreased from 100%-0% in a gradient mode; and meanwhile, the weight percentage of the 316H stainless steel is increased from 0-100% in a gradient manner. The gradient material is formed on a substrate by a laser additive process, so as to solve the problem that a part in a traditional welding mode is not suitable for the requirement of a lead or lead bismuth cooled reactor system, and is used for manufacturing parts of the lead or lead bismuth cooled reactor system.

Description

technical field [0001] The invention relates to the field of alloy materials, in particular to an alloy material for connecting dissimilar steels and a manufacturing method thereof. Background technique [0002] Ferritic martensitic steel and austenitic stainless steel, such as T91 and 316H, are commonly used in the manufacture of nuclear power reactor components. In traditional welding methods, nickel-based welding consumables are usually used for welding connections by surfacing welding. However, due to the high solubility of nickel in lead or lead-bismuth, this welded dissimilar structure is not suitable for nuclear test devices and fast neutron reactors cooled by lead or lead-bismuth. In addition, the traditional welding method forms a single transition zone at the welded joint of dissimilar steels, while ferritic martensitic steel and austenitic stainless steel have large differences in composition and microstructure. In this single transition zone, there are large comp...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F7/02B22F9/08B22F10/28B22F10/31B22F1/142B22F1/145B22F12/50C22C38/02C22C38/04C22C38/44C22C38/48C22C38/58B33Y10/00B33Y80/00
CPCB22F10/28B22F7/02B22F12/50B22F10/31B22F9/082C22C38/02C22C38/04C22C38/58C22C38/44C22C38/48C22C38/001B33Y10/00B33Y80/00Y02P10/25
Inventor 燕春光徐海涛李时磊李阳刘静
Owner CHINA INSTITUTE OF ATOMIC ENERGY