Curable resin composition, cured film, coated resin molded body and multilayer film
A technology of curable resin and resin composition, which is applied in the field of curable resin composition, cured film, resin-coated molding and multilayer film, and can solve the problems of dual curing and research.
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[0590] Hereinafter, the present invention will be described in more detail based on examples. In addition, this invention is not limited to the following Example. It should be noted that the parts herein represent weight.
Synthetic example 1
[0592] Mix 55 parts of ethylene glycol monoacetoacetate monomethacrylate, 66 parts of tert-butyl acrylate, 71 parts of potassium carbonate, 3 parts of 18-crown-6-ether, and 121 parts of tetrahydrofuran, and stir at 50°C for 3 hours . After completion of the reaction, cyclohexane and water were thrown in and washed with water. After the organic layer was neutralized with saturated ammonium chloride aqueous solution, it washed with water twice, and the obtained organic layer was concentrated under reduced pressure, and the monomer A was obtained.
Synthetic example 2
[0594] 55 parts of ethylene glycol monoacetoacetate monomethacrylate, 45 parts of methyl acrylate, 71 parts of potassium carbonate, 3 parts of 18-crown-6-ether, and 100 parts of tetrahydrofuran were mixed, and stirred at 50° C. for 3 hours. After completion of the reaction, cyclohexane and water were thrown in and washed with water. The organic layer was neutralized with saturated ammonium chloride aqueous solution, washed with water twice, and the obtained organic layer was concentrated under reduced pressure to obtain monomer B.
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Abstract
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