Thermal insulation material with fire resistance and preparation method thereof
A technology of thermal insulation material and fire resistance, applied in the direction of climate sustainability, sustainable waste treatment, solid waste management, etc., can solve problems such as fire spread, toxic smoke and molten droplets, and superior performance cannot make up for hidden safety hazards.
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Embodiment 1
[0017] Example 1: PVA-SiO 2 Preparation of the adhesive
[0018] PVA-SiO 2 The preparation method of the adhesive is: . Dissolve PVA in water to prepare a PVA solution with a volume fraction of 12%; .The Na 2 SiO 3 Add water to dissolve, and use citric acid to dissolve Na 2 SiO 3 The pH of the solution was adjusted to 11; PVA and Na 2 SiO 3 The weight ratio is 4:1; .The pH of 11 Na 2 SiO 3 The solution was added dropwise to the PVA solution at 60 °C, Na 2 SiO 3 The volume ratio of the solution to the PVA solution is 1:1. Stir while adding dropwise. After the dropwise addition is completed, continue stirring for 40 min until the pH value of the final mixed solution is 7, and then PVA-SiO can be obtained. 2 adhesive.
Embodiment 2
[0019] Example 2: PVA-SiO 2 Preparation of the adhesive
[0020] PVA-SiO 2 The preparation method of the adhesive is: . Dissolve PVA in water to prepare a PVA solution with a volume fraction of 12%; .The Na 2 SiO 3 Add water to dissolve, and use citric acid to dissolve Na 2 SiO 3 The pH of the solution was adjusted to 11; PVA and Na 2 SiO 3 The weight ratio is 5:1; .The pH of 11 Na 2 SiO 3 The solution was added dropwise to the PVA solution at 60 °C, Na 2 SiO 3 The volume ratio of the solution to the PVA solution is 1:1. Stir while adding dropwise. After the dropwise addition is completed, continue stirring for 50 min until the pH value of the final mixed solution is 9, and then PVA-SiO can be obtained. 2 adhesive.
Embodiment 3
[0021] Example 3: PVA-SiO 2 Preparation of the adhesive
[0022] PVA-SiO 2 The preparation method of the adhesive is: . Dissolve PVA in water to prepare a PVA solution with a volume fraction of 12%; .The Na 2 SiO 3 Add water to dissolve, and use citric acid to dissolve Na 2 SiO 3 The pH of the solution was adjusted to 11; PVA and Na 2 SiO 3 The weight ratio is 4.5:1; .The pH of 11 Na 2 SiO 3 The solution was added dropwise to the PVA solution at 60 °C, Na 2 SiO 3 The volume ratio of the solution to the PVA solution is 1:1. Stir while adding dropwise. After the dropwise addition is completed, continue stirring for 45 min until the pH value of the final mixed solution is 8, and then PVA-SiO can be obtained. 2 adhesive.
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