Water washing method for denim fabric and denim fabric
A denim fabric and washing technology, applied in chemical instruments and methods, dyeing methods, dry-cleaning fiber products, etc., can solve the problems of serious staining on the bottom surface and low color fastness, so as to improve color fastness and optimize the washing process , not easy to yellowing effect
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[0048] Further, the present application also provides a method for preparing an adsorbent. The adsorbent prepared by the following preparation method has a high adsorption rate for dyes. Specifically, it includes the following steps:
[0049] (2.1) Dissolve polyether ether ketone in sulfuric acid, and conduct sulfonation reaction at 70-90℃ for 110min-130min to obtain dark red viscous liquid. Slowly place the container with dark red viscous liquid on ice. In the distilled water mixture, heat is removed and the reaction is terminated to obtain a polymer, and the obtained polymer is washed with distilled water to make the pH value between 5.5-6, and the excess sulfuric acid in the polymer is removed; In, the mass concentration of the sulfuric acid adopted is 64%, the consumption of sulfuric acid can be 0.5-1L, and the polyetheretherketone of 80-150g is added in every 1L of sulfuric acid;
[0050] (2.2) Dissolve the polymer in dimethylformamide, at room temperature, stir in a mag...
Embodiment 1
[0074] Preparation of adsorbent: Dissolve 150g of polyetheretherketone in 1L of sulfuric acid, carry out sulfonation reaction at 80°C for 120min, slowly place the container with dark red viscous liquid in distilled water mixture containing ice, remove heat and Terminate the reaction, wash the obtained polymer with distilled water to make its pH value between 5.5-6, and remove the excess sulfuric acid in the polymer;
[0075] Dissolve 120 g of polymer in 1 L of dimethylformamide, stir at room temperature at 500 rpm in a magnetic stirrer for 1 h, then add 120 g of montmorillonite, stir the suspension in a magnetic stirrer, stir The speed was 350 rpm, the stirring time was 12 h, the centrifugal speed was 1200 rpm, and the centrifugal treatment time was 10 min. The sediment was retained, and after centrifugation, it was washed three times with distilled water, and finally dried at 40 °C to obtain the adsorbent.
[0076] Preparation of dye transfer inhibitor: firstly 60g mPEG500, 2...
Embodiment 2
[0084] The operation was the same as that of Example 1, except that no adsorbent was added in step (3).
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