Composite proton exchange membrane, preparation method thereof and fuel cell
A proton exchange membrane and proton exchange technology, applied in fuel cells, circuits, electrical components, etc., can solve the problems of large hydrogen permeation flux, short life, poor performance of membrane electrodes and fuel cells, etc.
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[0046] Correspondingly, based on the above composite proton exchange membrane, embodiments of the present invention also provide a method for preparing the composite proton exchange membrane. The process flow of the preparation method of the composite proton exchange membrane is as follows: figure 2 shown, including the following steps:
[0047] Step S01: Provide porous matrix membrane and proton exchange membrane
[0048] Step S02: forming graphene oxide and proton exchange membrane resin at least in the pores contained in the porous base membrane to form a reinforcing membrane;
[0049] Step S03 : laminating and combining the reinforcing membrane and the anode surface of the proton exchange membrane or the anode surface and the cathode surface respectively.
[0050] Wherein, the porous matrix membrane in step S01 is constituted as the porous matrix layer contained in the reinforcing layer 20 of the composite proton exchange membrane above or the porous matrix layer 23 ( ...
Embodiment A1
[0065] This embodiment provides a composite proton exchange membrane and a preparation method thereof.
[0066] The structure of the composite proton exchange membrane is as figure 1 As shown in (b), it includes a proton exchange base layer 10 and a reinforcement layer 20, wherein the reinforcement layer 20 includes a first reinforcement layer 21 and a second reinforcement layer 22, and the first reinforcement layer 21 is laminated and bonded to the anode surface 11 of the proton exchange base layer 10. Above, the second reinforcement layer 22 is laminated and bonded on the cathode surface 12 of the proton exchange base layer 10 . Wherein, the first reinforcement layer 21 and the second reinforcement layer 22 include a PTFE porous matrix layer (with a porosity of 70% and a pore size of 3 μm), and graphite oxide (carbon-to-oxygen ratio of 2:2) filled in the pores of the PTFE porous matrix layer. 1, with a size of 0.75 μm) and Nafion DC2020 proton exchange resin.
[0067] The ...
Embodiment A2- Embodiment A6
[0072] Embodiment A2 to embodiment A6 respectively provide a composite proton exchange membrane and a preparation method thereof.
[0073] The composite proton exchange membranes provided in Examples A2-A6 and their preparation process are basically the same as those in Example A1, except that the porosity of the porous matrix layer, that is, the reinforcing layer, is different, and the graphite oxide is replaced by graphene oxide. A2-Example A6 The porosity of the porous matrix layer, that is, the reinforcing layer in each example is shown in Table 2 below, respectively.
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