Raw solution of animal hair's protein for spinning regenerated fibres and its production method
A technology of regenerated fiber and spinning dope, applied in the direction of cellulose/protein conjugated artificial filament, conjugated synthetic polymer artificial filament, etc., can solve the problems of unusable old woolen fabrics and waste of limited natural resources, and achieve Excellent dyeability, strong price advantage, high economic and social benefits
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example 1
[0014] Example 1. Soak clean animal hair in 1.5% aqueous hydrogen peroxide solution for 70 minutes, then adjust the pH value to 10.5 with sodium hydroxide, slowly heat to 100°C, keep warm for 90 minutes, and cool down to 85°C , add 1.2% sodium bisulfite, keep warm for 40 minutes, and finally add 1% sodium ethanol sulfonate by protein weight to make the copolymerization at 75° C. for 40 minutes.
example 2
[0015] Example 2. Soak clean animal hair in 4% aqueous hydrogen peroxide solution for 40 minutes, then adjust the pH value to 9.5 with sodium hydroxide, slowly heat to 100°C, keep warm for 90 minutes, and cool to 85°C. Add 0.6% sodium bisulfite, keep it warm for 30 minutes, and finally add 5% sodium ethanol sulfonate by protein weight to make it copolymerize. The copolymerization temperature is 90° C. and the time is 70 minutes.
example 3
[0016] Example 3. Soak clean animal hair in 3% aqueous hydrogen peroxide solution for 65 minutes, then adjust the pH value to 10 with sodium hydroxide, slowly heat to 100°C, keep it warm for 90 minutes, and cool down to 85°C , add 0.9% sodium bisulfite, keep warm for 35 minutes, and finally add 3% sodium ethanol sulfonate by protein weight to make it copolymerize. The copolymerization temperature is 80° C. and the time is 60 minutes.
[0017] Synthesis of spinning dope:
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