Expanded grahpite/molybdenum disulfide composite solid lubricating material and its preparing process
A solid lubricating material, expanded graphite technology, applied in the petroleum industry, lubricating compositions, thickeners, etc., can solve the problem of unsatisfactory service life of molybdenum disulfide, achieve excellent solid lubricating performance, expand application scope, slow down The effect of tribo-oxidation
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[0029] Under laboratory conditions, expanded graphite was prepared chemically. Wherein, the raw material used is fine natural flake graphite with a particle size of 200 mesh and a purity of 99.9% (place of origin: Shandong Nanshu Graphite Company), the intercalation agent is concentrated sulfuric acid with a concentration of 98%, and the oxidizing agent is hydrogen peroxide with a concentration of 30%. Intercalation treatment at room temperature of about 25°C for 10 minutes, then the intercalated product was washed with water to a pH value of 8, then dried at 100°C for 2 hours, and subjected to high-temperature puffing treatment at a temperature of 900°C. An expanded graphite with an expansion factor of about 100 times is obtained.
[0030] The purity of the molybdenum disulfide powder used is 98.5%, the particle size is 0.8-5 μm, (place of origin: Tianjin Sifang Chemical Co., Ltd.), and the binder is epoxy resin.
[0031] First, the expanded graphite and molybdenum disulfide...
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