Method for cleaning, adsorbing bed by sucked air in sucking procedure in pressure varied adsorption

A technology of inhaling air and pressure swing adsorption, which is applied in the field of pressure swing adsorption, can solve the problems of incomplete desorption regeneration, decreased purity of purified gas, and reduced recovery rate of purified gas, and achieve the goal of improving regeneration effect, improving purity and high recovery rate Effect

Inactive Publication Date: 2006-07-05
SOUTHWEST RES & DESIGN INST OF CHEM IND
View PDF0 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, in the pressure swing adsorption device, the desorption and regeneration of components with a large amount of adsorption on the adsorbent are often incomplete, resulting in a decrease in the purity of the purified gas.
In the pressure swing adsorption process that requires high purity of the purified gas, the return part of the purified gas is used to flush the adsorption bed at the same time as the evacuation step, which can improve the purity of the purified gas, but the return of the purified gas will reduce the recovery rate of the purified gas by 5~ 30%

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for cleaning, adsorbing bed by sucked air in sucking procedure in pressure varied adsorption
  • Method for cleaning, adsorbing bed by sucked air in sucking procedure in pressure varied adsorption

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] The invention discloses a method for flushing an adsorption bed with inhaled air during the evacuation process of the pressure swing adsorption, and is used for removing ethylene from the mixed gas discharged from the air-conditioning fresh-keeping store.

[0017] As shown in the drawings, this embodiment adopts the usual adsorption bed A and adsorption bed B, and the pipelines 10, 20, 30, 40 and control valves 1A, 2A, 3A, 4A respectively connected to the adsorption bed A and adsorption bed B are configured. , 1B, 2B, 3B, 4B, wherein the control valves 4A, 4B are suction valves that respectively connect Tower A and Tower B with the atmosphere, and the vacuum pump D that communicates with control valves 3A and 3B constitutes a pressure swing adsorption system. The bed is packed with adsorbent activated carbon.

[0018] The pressure swing adsorption system operates under the control of a computer program, and the two adsorption beds alternately perform the adsorption proc...

Embodiment 2

[0021] A method of using inhaled air to flush the adsorption bed during the evacuation process of the pressure swing adsorption of the present invention. This embodiment adopts a pressure swing adsorption system similar to that of Example 1 with 4 adsorption beds. For 2000Nm 3 / h of nitrogen containing 15% carbon dioxide for purification. The adsorption pressure is 0.4MPa, and the pressure in the evacuation step is 0.03MPa. The adsorbent is activated carbon. The process steps of the four adsorption beds are continuously and alternately cycled: adsorption, pressure equalization, reverse pressure release, evacuation and suction air flushing (inhaled air volume 600Nm 3 / h), pressure equalization, boost. The carbon dioxide contained in the purified gas is <0.01%, and the nitrogen recovery rate is 98%.

Embodiment 3

[0023] A method of flushing the adsorption bed with inhaled air during the evacuation process of the pressure swing adsorption according to the present invention. This embodiment adopts a pressure swing adsorption system similar to that of Embodiment 1 with 4 adsorption beds. For 3000Nm 3 / h of nitrogen containing 10% carbon dioxide for purification. The adsorption pressure is 0.6MPa, and the vacuum step pressure is 0.02MPa. The adsorbent is 30% activated carbon + 60% fine-pore silica gel + 10% activated alumina. The process steps of the 4 adsorption beds cycled continuously and alternately are: adsorption, primary pressure equalization, secondary pressure equalization, reverse pressure release, evacuation and suction air flushing (inhalation air volume 350Nm 3 / h), secondary pressure equalization, primary pressure equalization, step-up. The treated purified gas contains carbon dioxide <0.005%, and the nitrogen recovery rate is 98.5%.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

A method for using the sucked air to flush the adsorption bed in the evacuation procedure of pressure-varying adsorption equipment, which has the adsorption bed filled by adsorbent, pipeline, control valve and vacuumizing pulp for selectively adsorbing some gas from the gas mixture to obtain the purified gas is disclosed. The pressure of adsorption bed in evacuation step is 0.05-0.007 MPa. The amount of sucked air is 5-50% of the gas mixture to be treated.

Description

technical field [0001] The invention relates to a pressure swing adsorption method for separation, impurity removal and purification of mixed gas, in particular to a method for evacuating and flushing an adsorption bed by sucking air in the evacuation process of the pressure swing adsorption method. Background technique [0002] The usual pressure swing adsorption method is carried out in a pressure swing adsorption device consisting of an adsorption bed filled with an adsorbent and its configuration pipelines and control valves. The pressure swing adsorption method utilizes the adsorption selectivity of the adsorbent to gas, and the characteristics of the adsorption capacity changing with pressure. . The adsorption capacity of the adsorbent increases when the pressure increases, and the adsorption capacity decreases when the pressure decreases. The regeneration of the adsorbent in the pressure swing adsorption process usually adopts the process of vacuum desorption regener...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & AuthorityPatents(China)
IPC IPC(8): B01D53/047
Inventor陈健张剑锋杨云蔺荣立
OwnerSOUTHWEST RES & DESIGN INST OF CHEM IND