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Production process of quarternary carbonate powder

A manufacturing process, carbonate powder technology, applied in the preparation of carbonate/acid carbonate, calcium carbonate/strontium/barium, rare earth metal compounds, etc., can solve the problem of uneven dispersion of scandium oxide and cathode emission current Density Inconsistencies, etc.

Inactive Publication Date: 2002-08-07
CAIHONG GRP ELECTRONICS CO LTD
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Problems solved by technology

However, the scandium oxide added in the above process is physically mixed with the ternary carbonate powder, and the scandium oxide is not uniformly dispersed, resulting in inconsistent cathode emission current density

Method used

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  • Production process of quarternary carbonate powder

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Embodiment Construction

[0043] Raw material proportioning of the present invention is as follows:

[0044] Barium nitrate 30g

[0045] Strontium nitrate 23 grams

[0046] Calcium nitrate 4 g

[0047] scandium oxide 1 g

[0048] Hydrochloric acid (concentration 20%) 6 grams

[0049] Sodium carbonate 30g

[0050] 0.7 liters of water

[0051] Manufacturing process of the present invention is as follows:

[0052] 1. Preparation of scandium chloride solution: add scandium oxide into hydrochloric acid with a concentration of 20% to react to form a scandium chloride solution.

[0053] 2. Preparation of nitrate solution: weigh barium nitrate, strontium nitrate, calcium nitrate and scandium chloride solution according to the above formula and add them into 80°C hot industrial pure water and stir to dissolve.

[0054] 3. Preparation of sodium carbonate solution: Dissolve sodium carbonate in 80°C hot industrial pure water...

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Abstract

The production process of quaternary carbonate powder includes the following steps: firstly, making scandium oxide and hydrochloric acid produce reaction to produce scandium chloride, then making thescandium chloride, barium nitrate, strontium nitrate, calcium nitrate and sodium carbonate produce coprecipitation reaction to obtain quaternary carbonate, then making the obtained quaternary carbonate undergo the processes of centrifugal filtering, washing, drying and sieving to obtain the invented finished product. Said product can be coated on the cathode, its transmitted current density can be raised by aboev once as compared with cathode coated with ternary carbonate.

Description

technical field [0001] The invention relates to a manufacturing process of quaternary carbonate powder composed of barium carbonate, strontium carbonate, calcium carbonate and scandium carbonate. The quaternary carbonate powder is mainly used as large-screen color picture tube and color display tube (hereinafter referred to as color tube) and can also be used to replace other cathode emitting materials for cathode ray tubes (CRT). Background technique [0002] The cathode is the heart part of the color tube. Its function is to emit electrons. These electrons are focused and accelerated by the electron gun and hit the fluorescent screen to stimulate the phosphor to emit light and form images that people can see. Usually, the cathode structure used in color tubes is shown in the accompanying drawings, and they are mainly composed of cathode sleeve (1), cathode cap or base metal (2), rare earth metal carbonate coating (3) and heating wire (4). The cathode casing (1) is provide...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B32/60C01F11/18C01F17/00H01J1/13
Inventor 窦秀英俞敏鱼卫芳贺群胜高岚
Owner CAIHONG GRP ELECTRONICS CO LTD
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