Method for pressure hydrothermal synthesis of MCM-41 mesoporous molecular sieve
A medium-porous molecular sieve, MCM-41 technology, applied in the direction of crystalline aluminosilicate zeolite, etc., can solve problems such as the inability to meet the requirements of catalytic process structural stability, achieve easy operation, improved thermal and hydrothermal stability, synthesis simple method effect
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Embodiment 1
[0016] The raw material is TEOS:H 2 O: CTACl: NaOH = 1.0: 130: 0.4: 0.4 molar ratio mixed and stirred evenly, then transferred to a polytetrafluoroethylene-lined autoclave, filled with 10.0MPa nitrogen, and then crystallized at 120 ° C for 48h, the The obtained product was filtered, washed with water and dried, and calcined at 550°C for 6 hours to remove the template agent, and then the molecular sieve was subjected to heat and hydrothermal treatment. The intensity retention rate of the XRD100 diffraction peak after treatment is shown in Table 1.
Embodiment 2
[0018] Press the raw material by Na 2 SiO 3 :H 2 O:CTAB:NH 3 ·H 2 The ratio of O=1.0:175:0.5:0.15 was mixed and then transferred to an autoclave, filled with 8MPa nitrogen, crystallized at 140°C for 35h, filtered, washed and dried, and then calcined at 650°C for 4h to remove the template agent. The data of molecular sieve after thermal and hydrothermal treatment are shown in Table 1.
Embodiment 3
[0020] The raw material is TEOS:H 2 O:CTAOH:NH 3 ·H 2 The ratio of O=1.0:40:0.08:0.25 was mixed and then transferred to the autoclave and filled with 14.5MPa nitrogen gas. After crystallization at 80°C for 72h, the product was filtered, washed and dried, and roasted at 500°C for 10h to remove the template agent, and then the molecular sieve After thermal and hydrothermal treatment, the results are shown in Table 1.
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