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448results about How to "Inhibition of adsorption" patented technology

Organosilicon type marine antifouling paint binder and preparation method and application thereof

The invention discloses organosilicon type marine antifouling paint binder. The structure of the paint binder is shown in the formula (1), wherein the paint binder is an organosilicon-polyurethane compound with bactericide side chain and R represents CH2CH3. The preparation method comprises the following preparation steps: 1) using chloropropylmethyldimethoxysilane and dimethyldimethoxysilicane to react and obtain chloropropyl-containing polysiloxane; 2) using chloropropyl-containing polysiloxane, tertiary amine and hydroxyl-containing tertiary amine to perform reflux reaction and generate polysiloxane with quaternary ammonium salt and hydroxyl; and 3) mixing isocyanate, butyltin dilaurate and polysiloxane with quaternary ammonium salt and hydroxyl with solvent, adding gamma-aminopropyltriethoxysilane to extend the chain and obtain prepolymer with the crosslinked group -Si(OCH2CH3), and using the prepolymer to perform crosslinking and condensation in the air and obtain the finished product. The organosilicon type binder has low surface energy performance and very good hydrophobicity; and the molecular chain has environmentally-friendly bactericide, thus the binder has very good bactericidal effect and marine antifouling effect.
Owner:ZHEJIANG UNIV

Polycrystalline silicon ingot casting process

The invention discloses a polycrystalline silicon ingot casting process. The process comprises the following steps: 1, preheating; 2, melting; 3, growing crystal: the temperature is controlled to T6 and is preserved for 1h, and T6=1420 DEG C; the hoisting height of a heat insulation cage is 90mm; the temperature is controlled to T6 and is preserved for 2h, and the hoisting height of the heat insulation cage is not changed; the temperature is controlled to T6 and is preserved for 3h, and the hoisting height of the heat insulation cage is 110mm; the temperature is gradually lowered from T6 to T7, the temperature lowering time is 7-9h, and the hoisting height of the heat insulation cage is 210mm; T7=1405 DEG C; the temperature is controlled to T7 and is preserved for 7-9h, and the hoisting height of the heat insulation cage is not changed; the temperature is controlled to T7 and is preserved for 7-9h, and the hoisting height of the heat insulation cage is not changed; the temperature is gradually lowered from T7 to T8, and the hoisting height of the heat insulation cage is not changed; T8=1395 DEG C; 4, annealing and cooling. The polycrystalline silicon ingot casting process has the advantages of simple steps, reasonable design, convenience in realization, easiness in grasp and good using effect and can reasonably control the ingot casting crystal growth process.
Owner:XIAN HUAJING ELECTRONICS TECH

Hydroxy-terminated hyperbranched polyamine-ester polymer and application thereof in microfluidic chip

The invention relates to hydroxy-terminated hyperbranched polyamine-ester polymer and an application thereof in a microfluidic chip. The preparation method of the hydroxy-terminated hyperbranched polyamine-ester polymer comprises the following steps: using equimolar diethanol amine and methyl acrylate to react and obtain N,N-dihydroxyethyl-3-aminomethyl propionate; and using trimethylolpropane and N,N-dihydroxyethyl-3-aminomethyl propionate to react, wherein G2 hydroxy-terminated hyperbranched polyamine-ester polymer, G3 hydroxy-terminated hyperbranched polyamine-ester polymer and G4 hydroxy-terminated hyperbranched polyamine-ester polymer are obtained respectively when the molar ratio of trimethylolpropane to N,N-dihydroxyethyl-3-aminomethyl propionate is 1:9, 1:21 or 1:45. The hydroxy-terminated hyperbranched polyamine-ester polymer is used to prepare the hydrophilic microfluidic chip. The preparation method of the chip comprises the following steps: oxidizing a polydimethylsiloxane (PDMS) microfluidic chip substrate in oxygen atmosphere; and connecting silane coupling agent with the inside of the substrate, and connecting the polymer with silane coupling agent. By strictly controlling the reaction conditions and the molar ratio of reactants, relatively regular polymer can be prepared. The polymer in the invention is used to modify PDMS, thus the hydrophilicity can be maintained permanent, any expensive instrument is not used and the preparation is convenient and fast.
Owner:UNIV OF JINAN
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