Blue luminophore for plasma fluorescent screen and its preparation method
A plasma and phosphor technology, applied in chemical instruments and methods, luminescent materials, solid cathode parts, etc., can solve problems that have not been solved stably, phosphors have poor chemical stability, are unstable and easy to hydrolyze, etc.
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[0030] Example 1, take the following reagent grade compounds respectively
[0031] Ba(OH) 2.8 h 2 O 0.89 mole
[0032] Eu 2 o 3 0.055 mole
[0033] Mg(OH) 2 1.00 mole
[0034] Al(OH) 3 h 2 O 9.60 mole
[0035] Sc(OH) 3 0.20 mole
[0036] Ga(OH) 3 0.20 mole
[0037] First, after heating the mixture of the above compounds to 100°C, the crystal water was evaporated and removed by a spray dryer with a rotation speed of 6000 rpm, and then ground by a star mill with a rotation speed of 2000 rpm.
[0038] Then, put the ground mixture into a crucible, and burn it in an atmosphere of nitrogen containing 5% hydrogen at a temperature of 1470° C. for 3 hours to obtain a chemical composition of Ba 0.89 Eu 0.11 MgAl 9.6 sc 0.2 Ga 0.2 o 17 of phosphors.
[0039] Finally, put the fired phosphor into a 1% concentration of metasilicate (H 2 SiO 3 ), and slowly add 0.2% magnesium acetate [Mg(CH 3 COO) 2 ] solution. T...
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