High transparent multi-layer coextrusion biaxially-oriented polyester film and its production method
A technology of biaxially stretching polyester and polyester film, applied in the field of packaging industry, which can solve the problems of high manufacturing cost and achieve the effects of good processability, low haze and high light transmittance
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Embodiment 1
[0031] The preparation of embodiment 1 polyester raw material
[0032]Two kinds of silicon dioxide with different particle sizes are mixed in ethylene glycol to prepare the ethylene glycol suspension of silicon dioxide. According to the conventional polymer synthesis method-direct polymerization method (PTA method) to produce polyester chips, first carry out Esterification reaction, then polycondensation reaction, before polycondensation, add ethylene glycol suspension containing silicon dioxide and polycondensation catalyst and stabilizer in the prior art, at 280 ° C, vacuum degree 10-66.7Pa, stirring speed 40rpm, The reaction time is between 2-3 hours, and mother slices are prepared. Mother slice M 1 (IV = 0.63) contains 3000ppm of Fuji Silicon S350 (particle size: 1.8μm), master chip M 2 (IV = 0.63) contained 2000 ppm of Fuji Silicon S350 (particle size: 1.8 μm) and 1000 ppm of Degussa OX-50 (particle size: 50 nm). The polyester chip raw materials used in the present inv...
Embodiment 2
[0034] Example 2 The performance test of biaxially stretched polyester film under different raw materials and parameters, and its comparison with the film structure and film performance of Comparative Example
[0035] In the present embodiment, a large amount of experimental data and experimental results are described, and the parameters of the biaxially stretched polyester film of the present invention are changed item by item and the resulting film properties are listed to prove the production of the biaxially stretched polyester film of the present invention. The optimal parameters required for stretching the polyester film, and the difference in structure and performance between the biaxially stretched polyester film of the present invention and the film of the comparative example can also be understood. E1-E7 described below is the experimental test of changing different raw materials and parameters to the three-layer co-extruded polyester film of the present invention; C1...
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