Process for preparing carbon-carbon precast member for carbon-carbon/aluminium composite material
A technology for aluminum composite materials and prefabricated parts, applied in the field of carbon-carbon prefabricated parts for carbon-carbon/aluminum composite materials, can solve the problems that affect the rapid development and application of carbon/aluminum composite materials, and have not yet seen carbon-carbon/aluminum composite materials. Aluminum composite materials and carbon fiber prefabricated parts are prone to deformation and other problems, achieving the effects of low cost, reduced deformation, and convenient production
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Embodiment 1
[0018] Embodiment 1: The prefabricated part skeleton material of the present embodiment adopts the polyacrylonitrile preoxidized fiber (PANOF) whole mat that prepares with acupuncture technology, and concrete process step is as follows:
[0019] a. Prepare polyacrylonitrile pre-oxidized fiber (PANOF) integral felt with a density of 0.21g / cm 3 ;
[0020] b. In the heat treatment furnace, heat the above-mentioned PANOF integral felt to 990°C for heat treatment, and keep it warm for 2 hours;
[0021] c. the above-mentioned heat-treated preform skeleton is placed in a chemical vapor infiltration furnace, with C 3 h 6 It is a precursor and is pyrolyzed under high temperature conditions. The pyrolysis temperature is 1000°C, the furnace pressure is 1333Pa, the gas flow rate is 500ml / min, and the pyrolysis time is 180 hours.
[0022] d. The above prefabricated parts are subjected to high temperature heat treatment in a high temperature heat treatment furnace, the heat treatment tem...
Embodiment 2
[0024] Embodiment 2: The prefabricated part skeleton of this embodiment adopts acupuncture process technology to prepare carbon fiber integral felt, and its specific process is as follows:
[0025] a. Prepare the above-mentioned carbon fiber integral felt with a density of 0.30g / cm 3 ;
[0026] b. In the heat treatment furnace, heat the carbon fiber integral felt to 980°C for heat treatment, and keep it warm for 2 hours;
[0027] c. Put the skeleton of the preform in the chemical vapor infiltration furnace to C 3 h 6 It is a precursor, the pyrolysis temperature is 1000°C, the furnace pressure is 1333Pa, the gas flow rate is 490ml / min, and the pyrolysis time is 180 hours.
[0028] d. The above-mentioned carbon-carbon preform is subjected to high-temperature heat treatment on the carbon-carbon preform in a high-temperature heat treatment furnace. The heat treatment temperature is 2300° C. and the temperature is kept for 3 hours.
[0029] Prepared by the above process, the de...
Embodiment 3
[0030] Embodiment 3: The prefabricated part skeleton of this embodiment adopts the acupuncture process technology to prepare the prefabricated part skeleton with alternate laminated structure of carbon fiber and fiber net, and its specific process is as follows:
[0031] a. Prepare the above-mentioned carbon fiber and fiber mesh alternately laminated structure, and its density is 0.47g / cm 3 ;
[0032] b. In the heat treatment furnace, heat the preform skeleton to 990°C for heat treatment and keep it warm for 2 hours;
[0033] c. Put the skeleton of the preform in the chemical vapor infiltration furnace to C 3 h 6 It is a precursor, the pyrolysis temperature is 1000°C, the furnace pressure is 1333Pa, the gas flow rate is 450ml / min, and the pyrolysis time is 170 hours.
[0034] d. The above-mentioned carbon-carbon preform is subjected to high-temperature heat treatment in a high-temperature heat treatment furnace at a heat treatment temperature of 2200° C. for 3 hours.
[00...
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