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Process of preparing mineral bonding material and its composite material with phosphate and aluminium-silicon material

A technology of mineral bonding materials and aluminum-silicon materials, which is applied to clay products, other household appliances, household appliances, etc., can solve the problems of reduced high temperature characteristics, coagulation and hardening of refractory castables, and low self-supporting strength. Effects of high temperature and durability, high mechanical strength

Inactive Publication Date: 2005-09-28
SOUTH CHINA UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] 3. The disadvantage of refractory castables that use phosphate as a chemical combination is that it is difficult to react with ordinary aluminum-silicon materials at room temperature. For this reason, MgO fine powder or aluminate cement is added to make the refractory castable harden (Han Xinglu edited
The introduction of these metal ions often causes the problem of lower high temperature characteristics of the system
The autotrophic strength of the latter two is low, and the main reaction process of the solid phase needs to be carried out under high temperature conditions.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] Example 1 Preparation of mineral bonding material

[0022] (1) Kaolin was calcined at 450°C for 48 hours to obtain metakaolin;

[0023] (2) The metakaolin obtained in step (1) is mixed with phosphate with a solid content of 55% by weight in a weight ratio of 40:10, and the mixture is poured into a mold for casting or compression molding, and after hardening at 30° C., a mineral bond with good durability is obtained. The material has a normal temperature compressive strength of 51MPa and a refractoriness higher than 1550°C.

[0024] The phosphate is composed of aluminum dihydrogen phosphate:aluminum monohydrogen phosphate=2:1 by weight.

Embodiment 2

[0025] Example 2 Preparation of mineral bonding material

[0026] (1) Kaolin is calcined at 940°C for 1 hour to obtain metakaolin;

[0027] (2) The metakaolin obtained in step (1) is mixed with ammonium dihydrogen phosphate with a solid content of 20% by weight in a weight ratio of 90:60, the mixture is poured into a mold for casting, and after hardening at 5° C., a mineral bonding material is obtained. The compressive strength at room temperature is 52MPa, and the refractoriness is higher than 1600°C.

Embodiment 3

[0028] Example 3 Preparation of mineral bonding material

[0029] (1) kaolin was calcined at 800°C for 6 hours to obtain metakaolin;

[0030] (2) The metakaolin obtained in step (1) is mixed with phosphate with a solid content of 30% by weight in a weight ratio of 60:50, the mixture is poured into a mold for casting, and after hardening at 100°C, a mineral bonded material is obtained. The compressive strength is 40MPa, and the refractoriness is higher than 1600°C.

[0031] The phosphate is composed of aluminum dihydrogen phosphate: aluminum monohydrogen phosphate: aluminum phosphate: aluminum polyphosphate=7:1:1:1 by weight.

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Abstract

The present invention relates to method of preparing mineral bonding material and its composite materials with phosphate and aluminum-silicon material at relatively low temperature. Under relatively low temperature, aluminum-silicon material with reaction activity is made to produce bonding reaction with phosphate to obtain one kind of amorphous solid Al-Si-P mineral bonding material. The Al-Si-P mineral bonding material may be used as basic material to prepare various composite materials with different performance via adding bauxite, silicon powder, flyash, mineral slag, fiber, etc. The said composite materials may be formed through casting or pressing, and the materials have excellent endurance, high mechanical strength and good high temperature performance.

Description

technical field [0001] The invention relates to the preparation technology of functional inorganic non-metallic materials such as high-temperature materials, corrosion-resistant materials and structural materials, in particular to a method for preparing mineral bonding materials and composite materials thereof from phosphate and aluminum-silicon materials. Background technique [0002] It is well known that the synthesis and preparation of solid-state materials often involve solid-state reactions. Traditional solid-state reactions need to be carried out under high temperature and high pressure conditions. However, under high temperature and other conditions, there are defects such as difficulty in controlling the macroscopic and microstructural characteristics of materials, low reaction speed, and unstable material properties. The technology of preparing solid materials by low-temperature solid-state reaction has become the direction that people pursue. [0003] The existin...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B33/04C04B33/13C04B33/36
Inventor 苏达根曹德光周新涛朱锦辉
Owner SOUTH CHINA UNIV OF TECH
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