Power-controlled bonding of resin or (co)polymer powder and flake materials
A technology of resin and power, which is applied in the field of manufacturing sticky powder, can solve the problems of inability to manufacture coating powder on an industrial scale, the appearance of the top coat is dark gray, and the coating cannot achieve gloss, so as to simplify the powder bonding method and reduce product failure High efficiency, reliable bonding effect
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Embodiment 1 and 2
[0068] The following examples represent possible uses of the invention, but are not actually practiced.
Embodiment 1
[0070] 4 pounds of acid functional polyester coating powder containing 10 phr (per 100 parts resin) of beta-hydroxyalkylamide curing agent was placed in a 5 liter Plasmec Turbomixer for Plastics, Model TRM-5. The mixer blades rotate at 1600 rpm. The power generated by the mixer is displayed and output to a programmable logic controller (PLC). Power initially increased to 6.5 watts, + / - 0.2 watts. As the powder reached its Tg, the power dropped to about 6.0 watts at 30 seconds, and then the power began to rise steadily above 6.5 watts. If the mixer continues to run, the powder will agglomerate into large clumps and the power watts will increase beyond the capability of that mixer, forcing the mixer to stop. Instead, the PLC intervenes when power reaches 7.2 watts (10% higher than the steady-state power initially produced). When the power reached 7.2 watts, the mixing paddle was slowed to 1000 rpm and 0.16 pounds of aluminum flake pigment was added to the mixer. The mixer wa...
Embodiment 2
[0072] 4 lbs of epoxy coating powder containing 10 phr of bisphenol A epoxy phenyl imidazole curing agent were placed in a 5 liter Plasmec turbo mixer, model TRM-5 for plastics. The mixer blades rotate at 1600 rpm. Display the power generated by the mixer and output to PLC. Power initially increased to 8 watts, + / - 0.2 watts. As the powder approaches its Tg, the power drops to about 7.6 watts at 30 seconds and then rises steadily above 8 watts. If the mixer continues to run, the powder will agglomerate into large clumps and the power watts will increase beyond the capability of that mixer, forcing the mixer to stop. Instead, the PLC intervenes when power reaches 8.8 watts (10% higher than the steady-state power initially produced). When the power reached 8.8 watts, the mixing paddle was slowed to 1000 rpm and 0.16 pounds of aluminum flake pigment was added to the mixer. The mixer was continued for 2 minutes at 1000 rpm. At the end of this cycle, the powder and aluminum fl...
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