Method for extracting series effective ingredient of pyracantha

A technology of active ingredients and extraction methods, which is applied in the field of extraction of active ingredients of Pyracantha series, can solve the problems of no comprehensive utilization research, single active ingredient, low resource utilization rate, etc., and achieve product safety, non-toxicity, low cost, The effect of high resource utilization

Inactive Publication Date: 2007-02-28
HUNAN AGRICULTURAL UNIV
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Problems solved by technology

However, since the 1990s, foreign research has mainly focused on the application of Pyracantha extract (active ingredient) in cosmetics, and has not yet involved research on pigments, pectin, food processing, etc.; domestic research has mainly focused on nutritional ingredients and medicinal ingredient analysis, food rough processing, etc., developed food and health products such as firebuckthorn fruit wine, beverages; but it has not yet involved important aspects such as the purification of red pigment and pectin, and the research and extraction is mainly a single active ingredient ( products), it does not involve the sequential extraction (co-production) of Pyracantha fruit juice, red pigment, yellow pigment, pectin and other active ingredients and the comprehensive utilization of residual pomace as feed raw materials, other important Pyracantha in Pyracantha The active ingredients are wasted in vain, the resource utilization rate is low, and the cost is high; as for the extraction method of the yellow pigment in the pyracantha fruit and the residual pomace as feed, there has been no report so far

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  • Method for extracting series effective ingredient of pyracantha

Examples

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Embodiment Construction

[0033] Figure 1 shows the process flow of the present invention.

[0034] Non-limiting examples of the invention:

[0035] (1) Take 100 kg of fresh Pyracantha japonicus fruit after removing impurities and cleaning, add 100 kg of water, squeeze and filter with a juicer, and obtain 128-131 kg of Pyracantha japonicus juice, which is used as a fruit juice drink after deastringent and sterilized or fruit wine, etc.; the pomace is used for the next step of extraction.

[0036] (2) In the pomace after squeezing the juice, add 500 kg of 65% ethanol aqueous solution with a pH of 3, heat extraction at 30-45°C for 40-50 minutes or ultrasonic extraction for 20-25 minutes or microwave extraction for 3 ~ 6 minutes, or cold soak for 18 ~ 22 hours, filter out the solution, and extract the filter residue twice in the same way. Combine the extracts obtained three times, recover ethanol under reduced pressure, purify with macroporous resin or silica gel column chromatography, spray dry or free...

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Abstract

The invention discloses an extracting method of effective ingredient of fire fruit series, which comprises the following steps: removing impurity, squeezing after cleaning, immersing to extract through acid low-grade alcohol, filtering, proceeding column chromatographic purifying, drying to obtain red coloring matter, adopting alcohol or acetone to extract fruit residual, filtering, recycling solvent, extracting, purifying, drying to obtain yellow coloring matter, utilizing alcaine to hydrolyze fruit residual, filtering, condensing, decolouring, sedimenting, purifying, drying to obtain pectin, making residuals as raw material of feed.

Description

technical field [0001] The present invention relates to a method for extracting active components of Pyracantha fruit series, specifically a method for sequentially extracting (co-producing) Pyracantha fruit juice, red pigment, yellow pigment, pectin and residual pomace from Pyracantha fruit as feed The method for raw materials belongs to the fields of preparation of food, food and cosmetic additives, active ingredients of natural products, and the like. Background technique [0002] Pyracantha fortuneana (Pyracantha fortuneana) is an evergreen wild shrub fruit tree plant in the genus Pyracantha Roem of the Rosaceae apple subfamily (Maloideae). In the southeast, southwest and northwest provinces of my country, it grows in mountains, hills, shrubs, grasslands and river ditches at an altitude of 500-2800m. Its peel is bright red (a few varieties are golden yellow). my country is extremely rich in Pyracantha resources. For example, Guizhou and Sichuan have an annual output of m...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L1/28A23L2/04A23K1/14A23K10/30A23L5/43A23L29/231
Inventor 熊远福蒋利华文祝友熊海蓉
Owner HUNAN AGRICULTURAL UNIV
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