Fuel additive composition suitable for control and removal of tenacious engine deposits
a technology of additive composition and engine, which is applied in the direction of fuel additive, liquid carbonaceous fuel, fuel additive, etc., can solve the problems of carburetor port, visible driveability, and automobile engine deposits on the surface of engine components, so as to prevent and control engine deposits
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example a3-1
Preparation of Dodecylphenoxy Poly(oxybutylene)poly(oxypropylene) Amine
[0093] A dodecylphenoxypoly(oxybutylene)poly(oxypropylene) amine was prepared by the reductive amination with ammonia of the random copolymer poly(oxyalkylene) alcohol, dodecylphenoxy poly(oxybutylene)poly(oxypropylene) alcohol, wherein the alcohol has a number average molecular weight of about 1598. The poly(oxyalkylene) alcohol was prepared from dodecylphenol using a 75 / 25 weight / weight ratio of butylene oxide and propylene oxide, in accordance with the procedures described in U.S. Pat. Nos. 4,191,537; 2,782,240; and 2,841,479, as well as in Kirk Othmer, “Encyclopedia of Chemical Technology”, 4th edition, Volume 19, 1996, page 722. The reductive amination of the poly(oxyalkylene) alcohol was carried out using conventional techniques as described in U.S. Pat. Nos. 5,112,364; 4,609,377; and 3,440,029.
example a3-2
Preparation of Dodecylphenoxy Poly(oxybutylene) Amine
[0094] A dodecylphenoxy poly(oxybutylene) amine was prepared by the reductive amination with ammonia of a dodecylphenoxy poly(oxybutylene) alcohol having an average molecular weight of about 1600. The dodecylphenoxy poly(oxybutylene) alcohol was prepared from dodecylphenol and butylene oxide, in accordance with the procedures described in U.S. Pat. Nos. 4,191,537; 2,782,240; and 2,841,479, as well as in Kirk Othmer, “Encyclopedia of Chemical Technology”, 4th edition, Volume 19, 1996, page 722. The reductive amination of the dodecylphenoxy poly(oxybutylene) alcohol was carried out using conventional techniques as described in U.S. Pat. Nos. 5,112,364; 4,609,377; and 3,440,029.
[0095] B. The Glycol Ether Component
[0096] The glycol ether employed in this invention can be represented by the formula:
R3—OR4OyH B-I [0097] wherein: [0098] R3 is a hydrocarbyl group having from about 1 to about 30 carbon atoms; [0099] R4 is a C2 to C5 a...
example c-1
Preparation of a 4-polyisobutylphenoxyethyl para-aminobenzoate
a) Polyisobutyl phenol
[0124] To a flask equipped with a magnetic stirrer, reflux condenser, thermometer, addition funnel and nitrogen inlet was added 203.2 grams of phenol. The phenol was warmed to 40.degree. C. and the heat source was removed. Then, 73.5 milliliters of boron trifluoride etherate was added dropwise. 1040 grams of Ultravis 10 Polyisobutene (molecular weight 950, 76% methylvinylidene, available from British Petroleum) was dissolved in 1,863 milliliters of hexane. The polyisobutene was added to the reaction at a rate to maintain the temperature between 22.degree. C. to 27.degree. C. The reaction mixture was stirred for 16 hours at room temperature. Then, 400 milliliters of concentrated ammonium hydroxide was added, followed by 2,000 milliliters of hexane. The reaction mixture was washed with water (3.times.2,000 milliliters), dried over magnesium sulfate, filtered and the solvents removed under vacuum to y...
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