Gel mould-injecting formation method of porous titanium with various shape
A technology of gel injection molding and complex shapes, which is applied in the field of powder metallurgy molding, which can solve the problems of difficult to obtain porous materials, high cost, and low porosity, and achieve uniform macroscopic distribution of pores, high-efficiency production, and high porosity. Effect
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Embodiment 1
[0016] The raw material of titanium powder is commercially available 50-100 μm titanium powder; acrylamide is produced by Tianjin Chemical Reagent Research Institute, which is a white fine crystal; N, N-methylenebisacrylamide is produced by Tianjin Kemiou Chemical Reagent Development Center, It is white powder.
[0017] Dissolve 15 grams of acrylamide and 1 gram of N,N-methylenebisacrylamide in 100 ml of water, add 450 grams of titanium powder and 5 grams of polyacrylic acid dispersant, and vacuum defoam for 30 minutes after ball milling to obtain a solid phase The slurry with a volume fraction of 50% is injected into the metal mold, and the mold is moved into an 80°C thermostat for 120 minutes. After demoulding, it is vacuum-dried for 72 hours to obtain the green body of the gel injection molded porous titanium part; the green body is sintered Get porous titanium parts.
[0018] The gel injection molded porous titanium parts prepared by this process had a porosity of 43.2% a...
Embodiment 2
[0020] The raw material of titanium powder is commercially available 50-100 μm titanium powder; acrylamide is produced by Tianjin Chemical Reagent Research Institute, which is a white fine crystal; N,N-methylenebisacrylamide is produced by Tianjin Kemiou Chemical Reagent Development Center, It is white powder.
[0021] Dissolve 20 grams of acrylamide and 6 grams of N,N-methylenebisacrylamide into 100 ml of water to make a solution, add 300 grams of titanium powder and 10 grams of polyacrylamide dispersant, and vacuum defoam for 20 minutes after ball milling for 24 hours , to prepare a slurry with a solid phase volume fraction of 40%. The resulting slurry is poured into a glass mold and kept at 60°C for 120 minutes. The slurry in the mold is solidified into a green body. After demoulding, it is vacuum-dried for 48 hours to obtain a gel-cast porous titanium part green body; the green body is sintered Get porous titanium parts.
[0022] The gel injection molded porous titanium ...
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