Dedicated nano compound agglomerate for outdoors lamp and its preparation method

A nano-composite, outdoor lighting technology, applied in the field of outdoor lighting materials, can solve the problem of not finding a special nano-composite masterbatch for outdoor lighting and other problems, achieve good thermal processing stability, reduce fracture reaction speed, improve dispersion and light stability. Effect

Inactive Publication Date: 2008-06-18
PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0011] However, there is no report on the application of inorganic nanoparticles to manufacture nanocomposite masterbatches for outdoor lamps with high weather resistance and no pollution to the environment.

Method used

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  • Dedicated nano compound agglomerate for outdoors lamp and its preparation method
  • Dedicated nano compound agglomerate for outdoors lamp and its preparation method
  • Dedicated nano compound agglomerate for outdoors lamp and its preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0062] The preparation of embodiment 1 masterbatch of the present invention

[0063] Table 1

[0064] Recipe Components

Nylon 6

Rutile nano-TiO 2

Irganox245

Ultranox626

Tinuvin770

calcium carbonate

Weight / (kg)

95.5

0.5

0.1

0.3

0.1

3.5

[0065] a. Take the materials as shown in Table 1;

[0066] b. Inorganic nanomaterials, rutile nano-TiO 2 Dry at 110°C for 3 hours, and vacuum-dry the polymer resin at 120°C for 15 hours;

[0067] c, the rutile nano-TiO 2 Pre-mix with polymer resin, inorganic fillers, and organic additives in a mixer for 4-8 minutes, and the pre-mixing speed is 1000-1500rpm;

[0068] d. Melt and extrude the pre-mixed material with twin-screw extrusion equipment with an aspect ratio greater than 40 at 230-290°C, the screw speed is 80-200rpm, and then cool the extruded material with water at a temperature of 70-160rpm Granulation is carried out at a rotating speed to form a w...

Embodiment 2

[0069] The preparation of embodiment 2 masterbatch of the present invention

[0070] Table 2

[0071] Recipe Components

Nylon 66

Rutile nano-TiO 2

Irganox245

Ultranox626

Tinuvin770

Titanium dioxide

Weight / (kg)

96.7

0.3

0.1

0.3

0.1

2.5

[0072] Get material such as table 2, preparation method is with embodiment 1;

[0073] The rutile nano-TiO used in this embodiment 2 It is rutile nano-TiO 2 Obtained by inorganic coating and organic treatment, the specific preparation method steps are as follows:

[0074] Inorganic coating process:

[0075] The mass content is 10% rutile nano-TiO 2 The suspension was sanded for 90 minutes, and then the suspension was made into nano-TiO 2 For slurry with a content of 2% to 10%, sodium silicate and sodium metaaluminate are used as silicon-coated and aluminum-coated additives, and sulfuric acid solution with a mass concentration of 10% is used as an auxiliar...

Embodiment 3

[0078] The preparation of embodiment 3 master batches of the present invention

[0079] table 3

[0080]

[0081] Get material such as table 3, preparation method is the same as embodiment 2; The rutile type nano-TiO used in this embodiment 2 With embodiment 2.

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Abstract

The invention provides nanometer complex particle, comprising aliphatic polyamide, inorganic nano material, mineral filler, and organic auxiliary agent. The invention also provides the preparing method, which is simple and easy control. The nanometer complex particle can be used for lamp body, lamp shade, finishing material and other outdoor lamp materials, and the materials have the obvious anti-photoageing, good weatherability and light environmental pollution.

Description

technical field [0001] The invention relates to a nanocomposite masterbatch, specifically, it is a nanocomposite masterbatch specially used for outdoor lamps prepared from aliphatic polyamide, inorganic nanomaterials, inorganic fillers and organic additives, and belongs to the field of outdoor lamp materials . Background technique [0002] Plastics are widely used outdoors because of their advantages such as light material, insulation, wear resistance, corrosion resistance, aesthetics, simple processing technology, and low cost. However, when plastics (belonging to polymer resins) are exposed to high-energy ultraviolet radiation for a long time in outdoor use, they will undergo photoaging and lead to degradation, and the degradation products will react with oxygen or other active components in the air, resulting in yellowing. Glossiness and physical and mechanical properties will be greatly reduced, which will eventually lead to a reduction in its actual service life [Zhou ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L77/00C08K9/06C08K3/36C08K5/5393C08K5/3435F21V15/02
CPCY02B20/72
Inventor 曹建军郭刚吴健春涂铭旌朱胜友黄婉霞
Owner PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP
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