Method of improving gas separation film penetration instrument
A technology of gas permeability and gas separation membrane, which is applied in the field of chemical engineering and can solve problems such as impact
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specific Embodiment approach 1
[0019] exist figure 2 In the process, the upper and lower sides of the flat polymer membrane or inorganic membrane 20 are respectively glued on the ring-shaped aluminum foil tape 19, a layer of filter paper is placed on the porous backing plate 22 and fixed in the middle depression of the lower cover 18 of the membrane pool with glue, and placed Replace the O-shaped gasket 23, and fix the upper cover 17 of the membrane pool and the lower cover 18 of the membrane pool with hexagonal screws.
[0020] exist figure 1 in, will figure 2 The membrane pool in is connected in the gas path with temperature control box, and the temperature of temperature control box 16 is set. Close valve 1, three-way valve 7 and 15 of the gas to be measured, open valve 8, and turn valve 15 to vacuumize. In order to prevent membrane breakage (inorganic membrane, such as carbon membrane, etc.) and deformation (polymer membrane, etc.), the downstream system should be excluded first. the air inside. A...
specific Embodiment approach 2
[0023] exist image 3 In the process, the two ends of the tubular membrane 28 are sealed with glue, and one end is fixed on the support 25 with glue, and O-shaped sealing gaskets 27 are respectively placed on the left and right sides of the support, and the lower cover 26 of the membrane tank is screwed into the upper cover 24 of the membrane tank and fixed.
[0024] exist figure 1 in, will image 3 The membrane pool in is connected in the gas circuit with thermostat, after controlling the temperature of thermostat 16. Close the test gas valve 1, three-way valve 7 and 15, open the valve 8, and turn the valve 15 to vacuumize. In order to prevent the membrane from being broken and deformed, the air in the downstream system is firstly removed. After the downstream pressure drops, close the valves 2 and 13, open the valve 5 and turn the valve 7 to vacuumize, vacuumize the upstream and downstream of the entire gas circuit, and use the vacuum gauge 4 to judge that the vacuum has ...
Embodiment 1
[0028] The thickness is 20μm with epoxy glue, and the effective penetration area is 4.15cm 2 The circular polyimide film is fixed in the membrane cell, adopts specific embodiment 1, has obtained this organic film to hydrogen (H 2 ): 2.2 Barrer (1 Barrer = 10 -10 cm 3 (STP).cm.cm -2 ·s -1 ·cmHg -1 ), carbon dioxide (CO 2 ): 1.1Barrer, oxygen (O 2 ): 0.18Barrer, nitrogen (N 2 ): 0.034Barrer; selectivity: H 2 / N 2 = 64.7, CO 2 / N 2 =32.4,O 2 / N 2 = 5.3.
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