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Drawing lube cooling oil of aluminum-coated red copper metal bar and its production

A lubricating cooling oil and bimetal technology, which is applied in the direction of lubricating compositions, petroleum industry, base materials, etc., can solve the problems of bad influence of heat treatment and annealing quality, oxidation and discoloration of the surface of the drawn workpiece, smoothness, brightness reduction, etc., to achieve Good chemical adsorption and physical adsorption, not easy to deteriorate, and the effect of improving the diameter reduction rate

Inactive Publication Date: 2007-09-05
DALIAN SANDAAOKE CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the drawing lubricating coolant for copper-clad aluminum bimetallic rods uses oil-based lubricants, but the formed lubricating film has poor adhesion and is easy to be squeezed out during the drawing process, so that the drawn wire is drawn after repeated drawing. , the friction coefficient between the surface of the drawn wire and the edge of the hole core increases sharply, which not only causes the surface of the drawn workpiece to oxidize and discolor, and the smoothness and brightness decrease sharply, but also aggravates the wear and tear on the mold and affects the service life of the mold; in addition, there are The problem of unsatisfactory cleaning performance is not only easy to stick a large amount of metal powder on the surface of the drawn wire and the edge of the hole core during the drawing process, resulting in a further increase in the friction coefficient between the two, but also to the after-drawing of the metal wire. Process heat treatment and annealing quality will have adverse effects,

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] a. Get raw material components, each raw material accounts for the percentage of total weight as follows:

[0035] Machine oil (No. 32, No. 10, No. 7) 20-30%, oleic acid 8-9%, tricresyl phosphate 20-30%, benzotriazole 0.8-0.9%, absolute ethanol 1-2% , phosphobutyl zinc base zinc salt (T202) 20-30%, poly-n-butyl vinyl ether (T601) 13.5-14.5%, fungicide (isothiazolinone) 0.2-0.3%, each raw material can be listed Choose arbitrarily within the value range, and the total value should be 100%;

[0036] b. Fully dissolve the benzotriazole with absolute ethanol for later use;

[0037] c. Add mechanical oil into the reaction kettle, heat to 80-90°C, start the agitator at a speed of 550-650 rpm, and add tricresyl phosphate and oleic acid in sequence, stir for 0.5-1.5 hours, then lower the temperature drop to 40-50°C;

[0038] d. Add the ethanol-soluble solution of benzotriazole described in step a and the bactericide to the mixed solution described in step b, continue to stir ...

Embodiment 2

[0042] a. Get raw material components, each raw material accounts for the percentage of total weight as follows:

[0043] Mechanical oil (No. 32, No. 10, No. 7) 25.3%, oleic acid 8%, tricresyl phosphate 20%, benzotriazole 0.9%, absolute ethanol 2%, thiophosphobutyl zinc base zinc salt (T202 ) 30%, poly-n-butyl vinyl ether (T601) 13.5%, fungicide (isothiazolinone) 0.3%;

[0044] b. Fully dissolve the benzotriazole with absolute ethanol for later use;

[0045] c. Add mechanical oil into the reaction kettle, heat to 90°C, start the agitator at a speed of 550 rpm, and add tricresyl phosphate and oleic acid in sequence, and after stirring for 0.5h, lower the temperature to 40°C;

[0046] d. Add the ethanol-soluble solution of benzotriazole described in step a and the bactericide to the mixed solution described in step b, continue to stir for 0.5h, stop stirring and drop to normal temperature;

[0047] e. Then add phosphobutyl zinc base zinc salt and poly-n-butyl vinyl ether in tu...

Embodiment 3

[0050] a. Get raw material components, each raw material accounts for the percentage of total weight as follows:

[0051] Machinery oil (No. 32, No. 10, No. 7) 24.5%, oleic acid 9%, tricresyl phosphate 30%, benzotriazole 0.8%, absolute ethanol 1%, thiophosphobutyl zinc base zinc salt (T202 ) 20%, poly-n-butyl vinyl ether (T601) 14.5%, fungicide (isothiazolinone) 0.2%;

[0052] b. Fully dissolve the benzotriazole with absolute ethanol for later use;

[0053]c. Add mechanical oil into the reaction kettle, heat to 80°C, start the agitator at a speed of 650 rpm, and add tricresyl phosphate and oleic acid in sequence, and after stirring for 1.5 hours, lower the temperature to 50°C;

[0054] d. Add the ethanol-soluble solution of benzotriazole described in step a and the bactericide to the mixed solution described in step b, continue to stir for 1.5h, and cool down to normal temperature naturally;

[0055] e. Then add phosphobutyl zinc base zinc salt and poly-n-butyl vinyl ether i...

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PUM

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Abstract

A dual-metal rod pulling lube cooling oil of copper aluminum-coated consists of motor oil 20-30wt%, oleic acid 8-9wt%, tritolyl phosphate 20-30wt%, benamide azole trinitride 0.8-0.9wt%, anhydrous alcohol 1-2wt%, sulfur-phosphorus butanoctyl-zinc salt 20-30wt%, poly-n-butyl vinyl ether 13.5-14.5wt% and bactericide 0.2-0.3wt%. The process is carried out by dissolving benamide azole trinitride by anhydrous alcohol, adding motor oil into reactor, heating to 80-90degree, adding into tritolyl phosphate and oleic acid successively, agitating at 550-650 / min for 0.5-1.5hrs, lowering temperature to 40-50degree, adding benamide azole trinitride ethanol solution and bactericide into mixed solution, agitating for 0.5-1.5hrs, cooling, adding into sulfur-phosphorus butanoctyl-zinc salt and poly-n-butyl vinyl ether successively and agitating at 25-35 / min for 0.5-1.5hrs. It has excellent finish degree and brightness.

Description

Technical field: [0001] The invention relates to a lubricating cooling liquid for drawing process and a production method thereof, in particular to a copper-clad aluminum bimetallic rod drawing lubricating cooling which can prevent oxidation and discoloration of the finished product of the drawn bimetallic rod and ensure surface smoothness and high brightness. Oils and methods of production. Background technique: [0002] The drawing process is a typical metal processing method. It is a plastic processing process that reduces the cross-sectional area of ​​the metal processing material through the die hole core under the action of drawing to obtain a high-precision, high-gloss wire or pipe. During the drawing process, due to the large amount of metal deformation and the continuous generation of new friction surfaces, lubricating coolant is required to lubricate and cool the metal material and mold. Especially the copper-clad aluminum bimetallic rod drawing process generally ...

Claims

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Application Information

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IPC IPC(8): C10M145/26C10M137/04C10M133/44C10M101/00C10N40/24
Inventor 潘德顺黄猛
Owner DALIAN SANDAAOKE CHEM
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