Method for continuously casting titanium alloy near single-crystal ingot by using electromagnetic cold crucible

An electromagnetic cold crucible and titanium alloy technology, which is applied in the field of preparation of titanium alloy single crystal ingots, can solve problems such as low material performance, alloy pollution, long solidification time, etc., and achieve the effect of improving comprehensive mechanical properties

Inactive Publication Date: 2008-02-13
HARBIN INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] In order to solve the problem that the existing directional solidification methods are not applicable to the preparation of titanium alloy single crystals, this is due to the high activity of titanium alloys, which makes processing, forming and preparation relatively difficult, and the container material is easy to pollute the alloy when preparing single crystals. , the accuracy of the chemical composition of the alloy is poor, and the chemical inclusions are easy to ero

Method used

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  • Method for continuously casting titanium alloy near single-crystal ingot by using electromagnetic cold crucible
  • Method for continuously casting titanium alloy near single-crystal ingot by using electromagnetic cold crucible

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Experimental program
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Example Embodiment

[0012] Embodiment 1: The steps of the method for preparing a near-single crystal ingot of titanium alloy in this embodiment are as follows:

[0013] Step 1, vacuumize the furnace body of the cold crucible electromagnetic restraint forming and directional solidification device, the vacuum degree is 0.05-1Pa, and then backflush argon to 300-400Pa;

[0014] In step 2, a titanium alloy material rod 1 is arranged inside the cavity of the water-cooled copper crucible 2 in the directional solidification device, and an induction coil 3 is arranged outside the water-cooled copper crucible 2. The number of turns of the induction coil 3 is 4, and the wire diameter is 8 mm. , distributed on the outer surface of the water-cooled copper crucible 2;

[0015] Step 3. The titanium alloy material rod 1 enters 2-5 mm of the induction coil 3 under the control of the directional solidification device. The upper end of the pulling rod 37 is provided with a titanium alloy base material 35, the diame...

Example Embodiment

[0018] Embodiment 2: The upper end of the pulling rod in this embodiment is provided with a titanium alloy base material 35, the diameter of the upper part of the titanium alloy base material 35 is 25-26 mm, the height is 20-20 mm, and the diameter of the lower part of the titanium alloy base material 35 is 29 mm. ~29.5mm, height is 15~18mm. The above data range is convenient for melting, leak proofing and solidification.

Example Embodiment

[0019] Embodiment 3: The diameter of the titanium alloy material rod 1 in this embodiment is smaller than the diameter of the cavity of the water-cooled copper crucible 2 .

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Abstract

A method of continuously founding the titanium alloy to be close to an single crystal ingot with a magnetic field belongs to a method of making the titanium alloy to be close to the single crystal ingot. The method solves the problem that the container material is easy to pollute the alloy and thus affect the physical and mechanical performances of the single crystal alloy during preparation of single crystal in the current directional solidification methods. The procedures of the invention are as follows: 1. vacuum pumping is conducted in a furnace (4), and then argon is re-charged. 2. induction coils (3) are arranged out of a water-cooled copper crucible (2), and spread on the outer surface of the water-cooled copper crucible (2). 3. a material rod (3) enters into the induction coils (3), the titanium alloy charge enters into the cavity of the water-cooled copper crucible (2), and the diameter of the upper part of the charge is small. 4. After heating, pulling is conducted, the feeding speed must strictly match with the pulling action; a rod enters into a crystallizer (9); the material rod forms close single crystal after pulling, and obtains the single crystal ingot after processing the outer layer. The invention realizes high-grade, high-efficiency, safety, special and low-cost single crystal preparation method for the titanium alloy material.

Description

technical field [0001] The invention relates to a preparation method of a titanium alloy single crystal ingot. Background technique [0002] A single crystal refers to a substance composed of a single grain, and the growth of the grain is properly controlled, and finally grows into a crystalline structure composed of one grain. Because the whole structure is one grain without grain boundary, it has better comprehensive performance or a certain unidirectional performance than directional solidification structure and polycrystalline structure. At present, single crystal materials are widely used [0003] Used in aerospace blades, semiconductor silicon electronic materials, magnetostrictive materials, GaAs crystal luminescent materials, intermetallic compounds and various metal-based and inorganic composite materials. Nickel-based single crystal materials are currently the main materials for manufacturing advanced aero-engine and gas turbine blades. In nickel-based single cr...

Claims

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Application Information

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IPC IPC(8): C22F1/14B22D27/20B21C37/04
Inventor 陈瑞润丁宏升郭景杰毕维生傅恒志
Owner HARBIN INST OF TECH
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