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348results about How to "Improve high temperature mechanical properties" patented technology

Secondary cooling method for reducing transverse cracks of corners of microalloy sheet billet

InactiveCN102861890AGrain refinementReduced proeutectoidAusteniteMechanical property
The invention relates to a secondary cooling method for reducing transverse cracks of corners of a microalloy sheet billet, which is characterized in that the cooling temperature of a casting blank is facilitated to reach a temperature for starting the transformation from gamma to alpha by controlling the secondary cooling speed at an earlier stage when the casting blank passes through a vertical section after being delivered out of a crystallizer; at the later stage, the cooling water quantity of the casting blank is reduced, potential heat produced by the solidification of the casting piece is used for reheating the casting piece, and the reheating temperature is controlled to make the casting blank reach more than an austenite phase changing temperature when the casting piece is delivered out of the vertical section; the entire process is under the transformation of gamma to alpha to gamma, so that crystal grains of a final transformation product are smaller; and after the casting blank leaves the vertical section, the casting blank enters the subsequent secondary cooling area in a slowly cooling mode. By optimizing the continuous-casting billet cooling mode, the crystal grains are refined, and second-phase particles in the steel are controlled, so that the high-temperature mechanical property of the casting blank can be improved, simpleness in operation is realized, and the transverse cranks on the surface of the casting blank can be effectively reduced.
Owner:WISDRI ENG & RES INC LTD

Directional TiAl-based alloy and preparation method thereof

The invention discloses directional TiAl-based alloy and a preparation method thereof. According to the atomic percentage, TiAl alloy components are expressed as Ti-(40-50)Al-aNb-bCr-cMo-dV-eMn, wherein in the formula, a, b, c, d, e are atomic percentages, a+b+c+d+e is less than or equal to 10, and the balance is Ti. The method for preparing the columnar crystal TiAl-based alloy includes the following steps that mother alloy is smelted through vacuum induction suspension, and a mother alloy cast rod is prepared through vacuum suction casting; an optical floating zone crystal growth system is adopted, argon is used as protection gas, the flow speed is 3-3.6L/min, the width of a regional heating zone is 6-6.7mm, heat treatment is performed on the TiAl-based alloy cast rod, the heating temperature is controlled to be 1250-1350 DEG C, the drawing speed is in the range of 3-13 micrometers per second, and the columnar crystal TiAl-based alloy is prepared. Compared with a directional solidification technology, in the preparation method, peritectic reaction is omitted, and therefore peritectic segregation is avoided; the problem that refractory metal and alloy, such as tungsten and molybdenum, with direction tissue cannot be prepared through the direction solidification technology can also be solved.
Owner:NANJING UNIV OF SCI & TECH

High-performance tungsten/steel composite material based on high-temperature application and preparation method thereof

The invention relates to a high-performance tungsten / steel composite material based on high-temperature application and a preparation method thereof and belongs to the technical field of preparation of composite materials. By adoption of the high-performance tungsten / steel composite material, the problems of large residual joint stress, low strength, poor heat resistance and high connection temperature in an existing tungsten / steel connector are solved. The high-performance tungsten / steel composite material is prepared from a tungsten-based layer, a titanium layer, a niobium layer, a nickle layer and a steel-based layer which are arranged in sequence and prepared by adopting a welding method. The high-performance tungsten / steel composite material is obtained by superposing the tungsten-based layer, the titanium layer, the niobium layer, the nickle layer and the steel-based layer in sequence according to the superposition mode of the tungsten-based layer, the titanium layer, the niobium layer, the nickle layer and the steel-based layer and carrying out vacuum diffusion bonding. The high-performance tungsten / steel composite material has the advantages that the room-temperature tensile strength is larger than or equal to 352MPa, and the tensile strength at the temperature of 650DEG C is larger than or equal to 338MPa; the structure design is reasonable, the process is simple, the large-scale application is convenient, and simultaneously, the high-performance tungsten / steel composite material can be widely applied in diffusion bonding of refractory metal and other dissimilar metal materials.
Owner:CENT SOUTH UNIV

Light-weight corundum-magnesia alumina spinel refractory material and a preparation method of same

The invention relates to a light-weight corundum-magnesia alumina spinel refractory material and a preparation method of same, wherein porous corundum-magnesia alumina spinel ceramic material granules are used as an aggregate, wherein ceramic material being 3-5 mm in granular size accounts for 10-18 wt%, ceramic material being 1-2.8 mm in granular size accounts for 25-30 wt%, and ceramic material being 0.1-0.8 mm in granular size accounts for 15-20 wt%; a substrate includes 12-18 wt% of porous corundum-magnesia alumina spinel ceramic material fine powder with nano-scale pore diameter, 12-20 wt% of corundum fine powder, 2-5 wt% of magnesite fine powder and 3-8 wt% of alpha-Al2O3 micropowder. The preparation method includes the steps of: 1) placing the aggregate in a vacuum stirrer, vacuumizing the stirrer, and adding a magnesium chloride solution which accounts for 3-8 wt% of the total weight of the aggregate and the substrate, stirring the mixture, and turning off the vacuumizing system; 2) adding the substrate, stirring the materials, shaping and drying the materials, and performing temperature maintenance at 1450-1650 DEG C, cooling the material to produce the refractory material. In the refractory material, diameters of pores are nano-scale, so that the refractory material is low in heat conductivity and high in strength, has high anti-medium erosion performance and excellent thermal shock resistance.
Owner:WUHAN UNIV OF SCI & TECH

Method for continuously casting titanium alloy near single-crystal ingot by using electromagnetic cold crucible

A method of continuously founding the titanium alloy to be close to an single crystal ingot with a magnetic field belongs to a method of making the titanium alloy to be close to the single crystal ingot. The method solves the problem that the container material is easy to pollute the alloy and thus affect the physical and mechanical performances of the single crystal alloy during preparation of single crystal in the current directional solidification methods. The procedures of the invention are as follows: 1. vacuum pumping is conducted in a furnace (4), and then argon is re-charged. 2. induction coils (3) are arranged out of a water-cooled copper crucible (2), and spread on the outer surface of the water-cooled copper crucible (2). 3. a material rod (3) enters into the induction coils (3), the titanium alloy charge enters into the cavity of the water-cooled copper crucible (2), and the diameter of the upper part of the charge is small. 4. After heating, pulling is conducted, the feeding speed must strictly match with the pulling action; a rod enters into a crystallizer (9); the material rod forms close single crystal after pulling, and obtains the single crystal ingot after processing the outer layer. The invention realizes high-grade, high-efficiency, safety, special and low-cost single crystal preparation method for the titanium alloy material.
Owner:HARBIN INST OF TECH

Spinel casting sand and preparation method thereof

InactiveCN104557062AMeet the requirements of refractorinessImprove high temperature mechanical propertiesSodium BentoniteThermal expansion
The invention discloses magnesium-aluminum spinel casting sand prepared by sintering bauxite raw material and industrial magnesium oxide and a preparation process of the magnesium-aluminum spinel casting sand. The magnesium-aluminum spinel casting sand comprises the following main raw materials: 72.9% of bauxite raw material, 98% of magnesium oxide and the like. The preparation process comprises the following steps: weighing bauxite and industrial magnesium oxide powder according to a stoichiometric ratio, adding an appropriate amount of binders, mixing the materials, performing wet grinding, drying, pelletizing in a pelletizing machine, finally putting into a silicon molybdenum rod box type furnace for sintering and performing heat preservation at 1,550 DEG C for 5 h, cooling with the furnace, and then screening to obtain the magnesium-aluminum spinel casting sand. The novel spherical sand prepared by the preparation process disclosed by the invention has the characteristics of high temperature resistance, high strength, low thermal expansion rate, good anti-sticking sand performance, good recycling performance, low production cost and environmental friendliness; in the application aspect, the magnesium-aluminum spinel casting sand is suitable for molding methods of water glass, resin, bentonite and the like, and is suitable for precision casting, expendable pattern casting, V process casting and polishing treatment of nonferrous metals.
Owner:TAIYUAN UNIVERSITY OF SCIENCE AND TECHNOLOGY +2

Ni-Co-Al-Cr-Fe series single crystal high-entropy high-temperature alloy and preparation method thereof

The invention discloses a high-entropy high-temperature alloy and a preparation method thereof, and belongs to the field of high-entropy alloys. The alloy comprises the following chemical components of, in percentage by atom, 35%-40% of Ni, 30%-35% of Co, 10%-13% of Al, 5%-10% of Cr, 5%-8.5% of Fe, 1%-2.5% of Ti, 1%-3% of Ta, 0.01%-1% of Mo, 0.01%-1% of W, 0-1% of Re, 0.02%-0.12 % of C, 0.002%-0.015% of B, 0.005%-0.12% of Hf, and 0.05%-0.15% of RE, wherein Al+Ti+Ta is greater than or equal to 14% and less than or equal to 16%, and RE is any one rare earth element of Ce, La and Y. The preparation process of the alloy comprises the following steps of weighing and matching alloy elements according to the molar ratio, putting the alloy elements into a smelting furnace for smelting, carrying out high-temperature refining and casting to obtain an alloy ingot, preparing a (001) oriented single crystal high-entropy high-temperature alloy bar by adopting a high-speed solidification Bridgeman method, and then performing solution treatment and secondary aging treatment on the alloy bar. The prepared alloy bar has good high-temperature strength and thermal corrosion resistance, and is a candidate material of a hot-end part of an aero-engine and an industrial gas turbine.
Owner:UNIV OF SCI & TECH BEIJING

High-temperature high-strength TiAl-Nb monocrystal and preparation method thereof

The invention discloses a high-temperature high-strength TiAl-Nb monocrystal and a preparation method thereof. Based on the atomic percent, the high-temperature high-strength TiAl-Nb monocrystal comprises the alloy components: Ti-(43-47) Al-(6-10)Nb-(0.1-1)(C, Si), and the balance of Ti. The preparation method comprises the following steps: smelting TiAl-Nb button-shaped master alloy ingot casting by using an electro-magnetic induction suspension method; preparing a cylindrical rod-shaped sample by means of differential pressure suction casting or gravity casting; directionally condensing the cylindrical bar by using an optical float-zone crystal growth system to guarantee that the heating power is between 65% and 70%, the growth velocity is 5-30mm / h, the relative rotation speed is 20-40r / min and the argon flow protection is carried out for 3-5L / min; finally obtaining a TiAl-Nb monocrystal test bar; and performing desegregation heat treatment on the TiAl-Nb monocrystal bar to finally obtain the monocrystal test sample. By adopting the TiAl-Nb monocrystal alloy material prepared by using preparation method disclosed by the invention, the alloy pollution caused by a traditional Bridgman directional condensation method can be effectively avoided, a solid-liquid interface shape during condensation is controlled by regulating the heating power so as to quickly obtain the TiAl-Nb monocrystal, and after the desegregation of the TiAl-Nb monocrystal, the high-strength TiAl-Nb monocrystal alloy of which the yield strength is 637MPa at a temperature of 900 DEG C, the elongation percentage is 8.1% and the ductile-brittle transition temperature is not lower than 900 DEG C can be obtained.
Owner:NANJING UNIV OF SCI & TECH

High-strength high-corrosion-resistance double-phase heat resistant steel

The invention belongs to the field of heat resistant stainless steel and relates to high-strength high-corrosion-resistance double-phase heat resistant steel. The high-strength high-corrosion-resistance double-phase heat resistant steel comprises 0-0.1% of C, 0.1-1.0% of Si, 0-0.5% of Mn, 12-25% of Cr, 15-22% of Ni, 0-4.0% of Mo, 1.0-6.0% of Al, 0.1-1.0% of Nb, 0-0.05% of B, not larger than 0.03% of P, not larger than 0.02% of S and the balance Fe. A preparation method is characterized in that the vacuum degree is strictly controlled to be smaller than or equal to 5 Pa in the smelting process, so that adverse influences of N and Al chemical compounds are avoided; a hammer forging manner is adopted, and the strain rate is controlled to be not smaller than 1s-1in the hot rolling process; and the reduction in a single pass is not smaller than 35%, and the second-phase size is controlled through rapid cooling. The high-strength high-corrosion-resistance double-phase heat resistant steel enables high-temperature corrosion resistance and high strength to be matched, and the comprehensive performance of the high-strength high-corrosion-resistance double-phase heat resistant steel is obviously higher than that of existing double-phase heat resistant steel when the high-strength high-corrosion-resistance double-phase heat resistant steel is used in a high-temperature corrosive environment.
Owner:ANYANG INST OF TECH
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