Alkali metal lanthanum bismuthate gallate infrared optical glass and method for making same
A metal lanthanum bismuth gallate, infrared optics technology, applied in the field of glass, can solve the problems of poor chemical stability of fluoride glass and sulfide glass, complicated production process, easy crystallization, etc., and achieve the effect of good chemical stability
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Embodiment 1
[0038] 1) The molar composition of each component is: 35% Bi 2 o 3 , 45% Ga 2 o 3 , 10% La 2 o 3 , 10%K 2 O;
[0039] 2) Take by weighing a total amount of 50 grams, and mix it uniformly in a mortar;
[0040] 3) Move the uniformly mixed powder in 2) to a platinum crucible, put it in an electric furnace and heat it to 1200°C, and keep it for 3 hours;
[0041] 4) Pour the melt into a stainless steel mold, cool it naturally, and then put it into a muffle furnace for annealing. The annealing process is controlled by a program, and the temperature is kept at 400°C for 24 hours, and then cooled to room temperature;
[0042] 5) The glass sample is cut, finely ground and polished into a 20×20×2 mm sample.
[0043] 6) Meticon Model 2010 Prism Coupler waveguide analyzer is used to test its refractive index to be 2.41.
[0044] 7) SDT Q600 thermogravimetric analyzer was used to test the thermal properties, and the difference ΔT between the crystallization temperature and the tra...
Embodiment 2
[0048] The molar composition of each component is: 40% Bi 2 o 3 , 42% Ga 2 o 3 , 8% La 2 o 3 , 10% Na 2 O;
[0049] According to the preparation method of Example 1, the temperature in step 3) is controlled at 1000° C. and kept for 5 hours; the annealing temperature in step 4) is 300° C. and kept for 20 hours. The refractive index of the obtained infrared optical glass is 2.414, the difference ΔT between crystallization temperature and transition temperature is about 130°C, its infrared transmittance is shown in Figure 2, and its infrared transmission range is from 0.46 μm to 7.2 μm.
Embodiment 3
[0051] The molar composition of each component is: 45% Bi 2 o 3 , 30% Ga 2 o 3 , 5% La 2 o 3 , 10%K 2 O, 10% Na 2 O;
[0052] According to the preparation method of Example 1, the temperature in step 3) is controlled at 1300° C. and kept for 2 hours; the annealing temperature in step 4) is 350° C. and kept for 30 hours. The refractive index of the obtained infrared optical glass is 2.42, and the difference ΔT between the crystallization temperature and the transition temperature is about 150°C. The infrared transmittance is shown in Figure 3, and its infrared transmission range is from 0.5 μm to 7.2 μm. The schematic diagram of the thermogravimetric test is shown in Figure 4.
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