Supercritical carbonic anhydride wall-breaking method for melissa powder

A technology of carbon dioxide and bee pollen, applied in the fields of natural product health care products and pharmaceuticals, can solve the problems of long time required for wall breaking, increase product cost, and cannot be popularized and used, and achieves easy operation, energy saving, and beneficial nutrients. saved effect

Active Publication Date: 2008-09-24
陕西康泰莱生物医药工程有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Using this method to break the wall, the pollen needs to be soaked into a liquid before it can be processed, and the operation is complicated
[0005] (4) Fermentation and enzymatic wall-breaking method (patent application numbers 03115992.3, 87104508, 91106215.7, 95103910.5, 98104558.8, 02106399.0) is a widely used method, which uses the abundant microorganisms of pollen itself or the enzymes produced by inoculating microorganisms to make The content of pollen is degraded, and the osmotic pressure increases to break the pollen wall. This method takes a long time to break the wall, and it is easy to be contaminated by bacteria during the fermentation process, which will affect the quality.
This method is more complicated to operate, and the pollen content af

Method used

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  • Supercritical carbonic anhydride wall-breaking method for melissa powder
  • Supercritical carbonic anhydride wall-breaking method for melissa powder
  • Supercritical carbonic anhydride wall-breaking method for melissa powder

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Vacuum-dry fresh bee pollen to a moisture content of 6.20%, take 300g of dried pollen and put it into a 1L extractor, and use carbon dioxide with a purity of 99% to boost the pressure of the extraction vessel to a pressure of 15MPa at the temperature of the extraction vessel at 35°C; After 5 minutes of pressure, open the exhaust valve of the extraction tank to quickly empty the carbon dioxide and collect the pollen. Electron microscopy showed that the pollen cells had been broken.

Embodiment 2

[0029] Weigh 300g of dried bee pollen and put it into a 1L extractor. Under the condition of the temperature of the extraction tank at 35°C, use carbon dioxide with a purity of 99% to boost the pressure of the extraction tank to 30 MPa; keep the pressure for 5 minutes and then open the exhaust valve of the extraction tank to quickly discharge Empty carbon dioxide and collect pollen. Electron microscopy showed that the pollen cells had been broken.

Embodiment 3

[0031] Vacuum-dry the fresh bee pollen until the water content is 6.20%, take 300g of the dried pollen and put it into the 11 extractor, and under the condition of the temperature of the extraction kettle at 40°C, use carbon dioxide with a purity of 99% to boost the pressure of the extraction kettle to 30MPa; After maintaining the pressure for 10 minutes, open the exhaust valve of the extraction tank to quickly empty the carbon dioxide; just take out the pollen. Electron microscopy showed that the pollen cells had been broken.

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Abstract

The invention discloses a method using supercritical carbon dioxide to perform bee pollen broken-face. Bee pollen is put in an extraction plant of supercritical carbon dioxide, to react for a certain time in supercritical carbon dioxide liquid at the proper pressure and temperature, a vent valve is opened to rapidly empty carbon dioxide, so that a pollen cell expands acutely due to larger pressure difference of the inside and the outside, thereby cracking. The method has the advantages that the operation is simple and convenient, the cost is low, the whole process is performed below 50 DEG C, the broken-face time does not exceed 30 minutes, the influence of the product by thermotropy is reduced, so that the active ingredient is preserved completely, at the same time, bacillus can be killed, the unification of the broken-face and the sterilization processes is realized, the broken-face ratio of the pollen cell is high, but the percentage of damage is low, and the inclusion still exists in a cracked pollen wall under the dry condition, thereby favoring the preservation of the nutritious content.

Description

technical field [0001] The invention belongs to the technical field of natural product health care products and pharmacy, relates to a method for breaking bee pollen walls, and can be widely used in industries such as biopharmaceuticals and health food. Background technique [0002] Bee pollen is a mass formed by processing the pollen collected by bees from honey-pollen source plants. Bee pollen is very rich in nutrients and almost contains all nutrients. It is a high-quality source of nutrition, not only rich in protein, sugar Lipids, vitamins, organic acids, minerals, nucleic acids, as well as enzymes and other biologically active substances, are known as "miniature nutrient banks". Thousands of years ago, in ancient countries such as China and Greece, people began to eat pollen and use it as medicine. With the development of science and technology and the deepening of research, the health care functions of bee pollen have been gradually discovered, such as the prevention...

Claims

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Application Information

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IPC IPC(8): A23L1/076A23L1/29A23P1/06A23L21/20A23L33/00A23P10/40
Inventor 孙丽萍徐响高彦祥张智武
Owner 陕西康泰莱生物医药工程有限公司
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