Zinc cathode of zinc-nickel secondary battery and method for coating oxide on zinc oxide surface
A secondary battery, surface coating technology, applied to battery electrodes, alkaline battery electrodes, circuits, etc., can solve the problems of low theoretical gram capacity of calcium zincate and reduced battery capacity
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[0011] A preparation method for a zinc negative electrode of a secondary zinc-nickel battery has the following steps:
[0012] (1) 70.5-80.5 parts by weight of zinc oxide whose surface is coated with oxide, 3-5 parts by weight of conductive agent and other compounds of zinc and metal compound additives of 13-35 parts by weight if necessary and 0.5- 1 weight part of the hydrophilic binder powder is mechanically mixed to obtain a negative electrode active material and a hydrophilic binder semi-finished mixture;
[0013] (2) dissolving the dispersant of 0.01-3 parts by weight in distilled water of 15-30 parts by weight;
[0014] (3) Add the mixture of negative electrode active material and hydrophilic binder semi-finished product obtained in step (1) to the solution obtained in step (2), and then add hydrophobic binder with a dry basis amount of 0.5-3 parts by weight under stirring. agent emulsion to obtain a uniform zinc negative electrode slurry fluid;
[0015] (4) Coating th...
Embodiment approach 1
[0018] 1 part by weight of soluble SnCl 2 2H 2 O was dissolved in 10 parts by weight of concentrated hydrochloric acid, diluted 20 times with distilled water, and then 99 parts by weight of zinc oxide was added under the condition of mechanical stirring, and stirred for 0.5-5 hours. Sn-coated surface can be prepared by drying 6 o 4 (OH) 4 of zinc oxide powder. Then put 0.02g of sodium tripolyphosphate in the beaker, add 28g of deionized water, place the beaker on an electric heating stirrer and stir slowly, after the sodium tripolyphosphate is completely dissolved, add 100g of calcium zincate, zinc powder and By Sn 6 o 4 (OH) 4 Coated zinc oxide, 2g of conductive graphite, 0.03g of carbon black and 1.0g of sodium carboxymethyl cellulose powder are uniformly mixed, added to the above beaker, fully stirred, and then 1.5g of styrene-butadiene rubber emulsion with a concentration of 50% is added , stirred to obtain a uniform negative electrode active material slurry, and t...
Embodiment approach 2
[0020] 10 parts by weight of soluble SnCl 2 2H 2 O was dissolved in 10 parts by weight of concentrated hydrochloric acid, diluted 20 times with distilled water, and then 90 parts by weight of zinc oxide was added under the condition of mechanical stirring, and stirred for 0.5-5 hours. Sn-coated surface can be prepared by drying 6 o 4 (OH) 4 of zinc oxide. Then put 0.02g of sodium tripolyphosphate in the beaker, add 28g of deionized water, place the beaker on an electric heating stirrer and heat and stir slowly. After the sodium tripolyphosphate is completely dissolved, add 100g of calcium zincate and zinc powder and by Sn 6 o 4 (OH) 4 Coated zinc oxide, 2g of conductive graphite, 0.03g of carbon black and 1.0g of sodium carboxymethyl cellulose powder are uniformly mixed, added to the above beaker, fully stirred, and then 1.5g of styrene-butadiene rubber emulsion with a concentration of 50% is added , stirred to obtain a uniform negative electrode active material slurry...
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