Manchurian walnut bark extract and preparation method thereof
A technology of walnut bark and extract, which is applied in the field of walnut bark extract - catalpain and its preparation, and can solve problems such as easy recurrence
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Embodiment 1
[0017] The preparation method of walnut catalpa bark extract is to get 100kg of walnut catalpa bark and grind it into 50-60 mesh coarse powder (or broken into small pieces), add 6-8 times of drinking water, heat and extract three times, the temperature is 100 ℃, each time After 3 hours, filter, concentrate under reduced pressure at 50-60°C to a mother liquor containing 0.5-1g of medicinal material per 1ml, separate and purify with a macroporous adsorption resin, and obtain 200mg of brown-yellow walnut bark extract oil, with a yield of 2‰.
Embodiment 2
[0019] The preparation method of walnut catalpa bark extract is to get walnut catalpa bark 100kg and grind into 40-50 order coarse powder (or be broken into fritters), add 6 times amount of ethanol, ethanol concentration is 70%, heating and refluxing three times, heating temperature is 80-90°C, 1 hour each time, filter, concentrate under reduced pressure at 50-60°C to the mother liquor containing 0.5-1g of medicinal materials per 1ml, separate and purify by macroporous adsorption resin, and obtain 200mg of brown-yellow walnut bark extract oil , the yield is 2‰.
Embodiment 3
[0021] The preparation method of walnut catalpa bark extract is to take 100kg of walnut catalpa bark and grind it into coarse powder (or break into small pieces), add 7 times the amount of ethanol, the ethanol concentration is 80%, heating and refluxing three times, the heating temperature is 80-90 ° C , filtered for 1 hour each time, concentrated under reduced pressure at 50-60°C to a mother liquor containing 0.5-1g of medicinal material per 1ml, separated and purified by macroporous adsorption resin, to obtain 250mg of brown-yellow walnut bark extract oil, with a yield of 2.5‰.
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