Catalyst for removing nitrogen oxide in FCC stack gas at low temperature and production method thereof
A technology for regenerating flue gas and nitrogen oxides, which is applied in the field of catalysis and can solve problems such as poor removal activity
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Embodiment 1
[0020] ① Take 100g Fe 2 o 3 , 30g MnO 2 , 30g CuO kneaded evenly; ②Roast the kneaded material at 300℃~450℃ for 2h~4h; ③Put the roasted material in a colloid mill and add an appropriate amount of water to grind it into a stable slurry with good fluidity; Immerse 100g cordierite honeycomb carrier in the above slurry for 0.5h~1h, take it out and dry it at 100℃~120℃ for more than 12h, and then bake it at 300℃~450℃ for 2h~4h; ⑤Repeat step ④until the weight of the carrier increases by 20g , the prepared catalyst I.
Embodiment 2
[0022] ①Take 100g TiO2 2 , 30g Cr 2 o 3 , 30g CuO kneaded evenly; ②Roast the kneaded material at 300℃~450℃ for 2h~4h; ③Put the roasted material in a colloid mill and add an appropriate amount of water to grind it into a stable slurry with good fluidity; Immerse 100g cordierite honeycomb carrier in the above slurry for 0.5h~1h, take it out and dry it at 100℃~120℃ for more than 12h, and then bake it at 300℃~450℃ for 2h~4h; ⑤Repeat step ④ until the weight of the carrier increases by 40g , the prepared catalyst II.
Embodiment 3
[0024] ① Take equivalent to 100g Fe 2 o 3 of ferric nitrate, equivalent to 20g MnO 2 Manganese nitrate equivalent to 30g CuO and copper nitrate equivalent to 30g CuO were dissolved in water to prepare a mixed solution; ②Immerse 100g cordierite honeycomb carrier in the above solution for 0.5h~1h, take it out and dry it at 100℃~120℃ for more than 12h, then Calcining at 300°C-450°C for 2h-4h; ③repeating step ②until the weight of the carrier increases by 40g, and the prepared catalyst III is obtained.
[0025] The above-mentioned catalysts were packed in a fixed-bed reactor (filling volume: 2 mL) for activity determination. Feed containing NO500ppm, O 2 3%, n (NH3) / n (NO) 1.0 feed gas (N 2 For the balance gas), the reaction space velocity is 5000h -1 , the reaction pressure is 0.1MPa, and the reaction temperature is 180°C-300°C for NO selective catalytic reduction reaction, and the NO content in the inlet and outlet gas of the reactor is detected online with a trace NO ana...
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