Microcapsule aqueous suspension of phytocide clomazone and method of producing the same
The technology of clomazone and microcapsules is applied in herbicides and algaecides, botanical equipment and methods, biocides, etc., and can solve the problems of wall material not easily degradable, harming adjacent sensitive crops, complicated preparation process, etc. Achieve the effect of reducing pesticide loss and decomposition, improving pesticide stability, and simple preparation process
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[0042] The preparation method of embodiment 1-embodiment 5 is carried out according to the following step sequence:
[0043] a. Preparation of emulsion: Take sodium carboxymethylcellulose and gum arabic, add appropriate amount of deionized water, dissolve, add clomazone, emulsifier, antifoam agent, and emulsify homogeneously at a speed of 3000-10000r / min for 5 -30min, get stable oil-in-water emulsion A;
[0044] b. Complex coacervation: take gelatin, add an appropriate amount of deionized water to dissolve, and obtain aqueous solution B, mix B and A evenly, and adjust the pH value of the mixture of B and A to 3-4.5 with 10% acetic acid at a temperature of 35-55°C. React at constant temperature for 40-60min to form reactant C;
[0045] c. Curing: Cool the reactant C to a temperature of 0-5°C, adjust the pH value to 8-10 with 20% sodium hydroxide solution, add a curing agent, and cure for 40-60 minutes; the temperature rise rate is slow at 1°C per minute Raise the temperature ...
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