Big magnetostriction alloy with high mechanical strength and manufacturing method thereof
A technology of magnetostriction and mechanical strength, applied in the direction of material selection for magnetostrictive devices, device material selection, etc., can solve problems such as restricting the application of magnetostrictive materials, large saturation magnetization field, and difficulty in single crystal preparation, etc. Achieve the effect of being beneficial to mass production, grain refinement and low cost
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Embodiment 1
[0022] 1) Mn and Fe with a purity greater than 99.5wt% are used as raw materials, weighed at an atomic percentage of 40:60 and placed in a quartz crucible, and the vacuum degree of the vacuum chamber is adjusted to 5×10 -2 ~2×10 -3 Pa, into high-purity argon as protective gas, intermediate frequency induction heating and melting, and cast in a water-cooled copper mold to form a rod-shaped Mn with a cross-section of 10mm thick × 12mm wide 40 Fe 60 alloy ingot.
[0023] 2) The smelted rod-shaped Mn 40 Fe 60 The alloy ingot was heated to 900°C in a vacuum tube furnace for 72 hours to homogenize its composition, and then slowly cooled to room temperature.
[0024] 3) For homogenized rod-shaped Mn 40 Fe 60 The alloy was cold-rolled 6 times, with a reduction of 0.5 mm each time. In order to eliminate cold work hardening, it was annealed at 300 ° C for 2 hours, and then rolled 4 times to obtain a rolling rate of 50%. 40 Fe 60 Alloy cold-rolled plate, thickness 5mm.
[0025] ...
Embodiment 2
[0031] 1) Mn and Fe with a purity greater than 99.5wt% are used as raw materials, weighed at an atomic percentage of 50:50 and placed in a quartz crucible, and the vacuum degree of the vacuum chamber is adjusted to 5×10 -2 ~2×10 -3 Pa, into high-purity argon as protective gas, intermediate frequency induction heating and melting, and cast in a water-cooled copper mold to form a rod-shaped Mn with a cross-section of 10mm thick × 12mm wide 50 Fe 50 alloy ingot.
[0032] 2) The smelted rod-shaped Mn 50 Fe 50 The alloy ingot was heated to 900°C in a vacuum tube furnace for 100 hours to homogenize its composition, and then slowly cooled to room temperature.
[0033] 3) For homogenized rod-shaped Mn 50 Fe 50 The alloy cast rod is cold-rolled 5 times, each reduction is 0.5mm, in order to eliminate cold work hardening, it is annealed at 300°C for 0.5h, rolled for 6 passes, annealed at 300°C for 3h, and finally Re-rolling for 5 passes to obtain Mn with a rolling ratio of 80% 50...
Embodiment 3
[0040] 1) Mn and Fe with a purity greater than 99.5wt% are used as raw materials, weighed according to the atomic percentage of 55:45 and put into a quartz crucible, and the vacuum degree of the vacuum chamber is adjusted to reach 5×10 -2 ~2×10 -3 Pa, into high-purity argon as protective gas, intermediate frequency induction heating and melting, and cast in a water-cooled copper mold to form a rod-shaped Mn with a cross-section of 10mm thick × 12mm wide 55 Fe 45 alloy ingot.
[0041] 2) The smelted rod-shaped Mn 55 Fe 45 The alloy ingot is heated to 1000°C in a vacuum tube furnace for 24 hours to homogenize its composition, and then slowly cooled to room temperature.
[0042] 3) For homogenized rod-like Mn 55 Fe 45 The alloy ingot was cold-rolled for 5 passes, with a reduction of 0.5mm each time. In order to eliminate cold work hardening, it was annealed at 300°C for 0.5h, rolled for 6 passes, annealed at 300°C for 5h, and finally Re-rolling for 5 passes to obtain Mn wi...
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