Extreme-pressure lubricating grease and preparation method thereof
A lubricating grease and extreme pressure technology, applied in the field of lubricating grease, can solve the problems that the lubricating grease is difficult to meet the lubrication requirements of heavy-duty equipment, the moving parts are sintered together, and the equipment lubrication fails, so as to achieve good high temperature performance and improve load bearing capacity , Improve the effect of extreme pressure performance
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example 1
[0026] Add 90 grams of MDI to 1500 grams of autoclave oil, heat to 60°C, add 45 grams of octylamine and 35 grams of aniline to 600 grams of oil, heat to 60°C, and mix well (these three raw materials are passed through chemical reaction to generate component B), add 51 grams of stearic acid, 26 grams of benzoic acid, 18.4 grams of triisopropoxy aluminum, rise to 90 ° C, keep the temperature for 1 hour (these three raw materials react at a certain temperature to form group A 1 minute), continue heating to 120°C, add 6.5 grams of tap water, and keep the temperature constant for 1 hour (during this process, component B and component A further react to form a new type of grease composition), continue to heat the material to 160°C, and keep the temperature constant for 10 Minutes (the new grease composition is further stabilized), add 700 grams of quenching oil, and when the temperature drops below 120°C, sequentially add 15.2 grams of diphenylamine, 30.2 grams of vanlube829, and 30....
example 2
[0041] Add 90 grams of MDI to 1500 grams of autoclave oil and heat to 80°C. At the same time, add 66.8 grams of dodecylamine and 34.6 grams of cyclohexylamine to 600 grams of oil and heat to 80°C. Mix well and add hard 102 grams of fatty acid, 58.8 grams of methyl-benzoic acid, 73 grams of aluminum isopropoxide, constant temperature for 1 hour, continue to heat to 100 ° C, add 26 grams of tap water, constant temperature for 1 hour, continue to heat up the material to 170 ° C, constant temperature for 0.5 hours , 700 grams of accelerated cooling oil, when the temperature drops to 120 ° C, sequentially add 22.6 grams of N-phenyl-α-naphthylamine, 48.4 grams of vanlube8294, and 38.7 grams of dodecenylsuccinic acid, and carry out after stirring. Processed finished fat. Carry out aftertreatment after stirring evenly, the lubricating grease performance that the present invention's process formula makes is listed in table 2
[0042] Table 2
[0043] Pilot projects
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example 3
[0056] Add 28.4 grams of TDI to 2600 grams of autoclave oil and heat to 100°C. At the same time, add 48.5 grams of octadecylamine and 19.3 grams of p-toluidine to 600 grams of oil and heat to 100°C. Mix well and add hard 77 grams of fatty acid, 39 grams of benzoic acid, 55 grams of aluminum isopropoxide, at 100 ° C, constant temperature 1.2 hours, continue to heat to 140 ° C, add 14.6 grams of tap water, constant temperature 1.5 hours, continue to heat up the material to 190 ° C, constant temperature 30 Minutes, 680 grams of rapid cooling oil, when the temperature dropped to 110 ° C, sequentially added 17.6 grams of diphenylamine, 17.6 grams of 2,6-di-tert-butyl-p-cresol, 70.5 grams of vanlube972, and 35.2 grams of barium dinonylnaphthalenesulfonate, After stirring evenly, post-processing is carried out to obtain the finished fat. The performance of the lubricating grease that process formula of the present invention makes is listed in table 3
[0057] table 3
[0058] ...
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