Electrolytic manganese slag microcrystalline glass and preparation method thereof
A technology for electrolytic manganese slag and glass-ceramic, applied in the field of glass-ceramic, can solve the problems of complicated production process, unfavorable for popularization and application, many components, etc., and achieves the advantages of environmental protection, outstanding energy saving effect and simple method. Effect
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Embodiment 1
[0035] The composition and mass percent of the raw material of a kind of electrolytic manganese slag glass ceramics are:
[0036] Electrolytic manganese slag: 75%
[0038] Quartz sand: 10%
[0039] Magnesium Carbonate: 5%.
[0040] The concrete steps of a kind of preparation method of electrolytic manganese slag glass ceramics are as follows:
[0041] (1) Basic glass melting
[0042] Using electrolytic manganese slag, calcium carbonate, quartz sand, and magnesium carbonate as raw materials, first stir it according to the mass percentage of electrolytic manganese slag: calcium carbonate: quartz sand: magnesium carbonate: 75%: 10%: 10%: 5% Evenly, put the raw material mixture into the kiln for melting, the melting temperature is 1400°C, and the melting time is 30 minutes, and the basic glass melt of electrolytic manganese slag is melted.
[0043] (2) Basic glass molding
[0044] After the first step (1) is completed, the electrolytic mangane...
Embodiment 2
[0050] The composition and mass percent of the raw material of a kind of electrolytic manganese slag glass ceramics are:
[0051] Electrolytic manganese slag: 99.7%
[0052] Calcium carbonate: 0.1%
[0053] Quartz sand: 0.1%
[0054] Magnesium Carbonate: 0.1%.
[0055] The concrete steps of a kind of preparation method of electrolytic manganese slag glass ceramics are as follows:
[0056] (1) Basic glass melting
[0057] Same as Example 1, wherein: the mass percent of electrolytic manganese slag: calcium carbonate: quartz sand: magnesium carbonate is 99.7%: 0.1%: 0.1: 0.1%, the melting temperature is 1300° C., and the melting time is 45 minutes.
[0058] (2) Basic glass molding
[0059] Same as Example 1, wherein: the thickness of the base glass tiling is 20 mm.
[0060] (3) Nucleation and crystallization treatment
[0061] Same as Example 1, wherein: the glass nucleation temperature is 750° C., the nucleation time is 1 hour, the crystallization temperature is 1050° C.,...
Embodiment 3
[0065] The composition and mass percent of the raw material of a kind of electrolytic manganese slag glass ceramics are:
[0066] Electrolytic manganese slag: 90%
[0067] Calcium Carbonate: 8%
[0068] Quartz sand: 0.2%
[0069] Magnesium Carbonate: 1.8%.
[0070] The concrete steps of a kind of preparation method of electrolytic manganese slag glass ceramics are as follows:
[0071] (1) Basic glass melting
[0072] Same as Example 1, wherein: the mass percent of electrolytic manganese slag: calcium carbonate: quartz sand: magnesium carbonate is 90%: 8%: 0.2%: 1.8%, the melting temperature is 1350 ° C, and the melting time is 60 minutes.
[0073] (2) Basic glass molding
[0074] Same as embodiment 1, wherein: the thickness of the base glass tiling is 30 mm.
[0075] (3) Nucleation and crystallization treatment
[0076] Same as Example 1, wherein: the glass nucleation temperature is 725° C., the nucleation time is 1.5 hours, the crystallization temperature is 1080° C., ...
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