Polylactide metal fiber
A metal fiber, polylactic acid technology, applied in the direction of fiber chemical characteristics, conjugated synthetic polymer rayon, conjugated rayon, etc., can solve the limitations of processing and application, low melting point, high molecular weight polyester synthesis difficulties, etc. problem, to achieve the effect of good mechanical strength
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[0013] Synthesis of high-molecular-weight polylactic acid: the raw material is lactide, the catalyst is stannous chloride, and the amount of stannous chloride is 600×10 of the lactide amount -6 , the continuous polymerization process is completed through four reactors, and the synthesis process of polylactic acid:
[0014] condition
Reactor I
Reactor II
Reactor III
Reactor IV
140~150
160~180
230~240
230~240
Reaction pressure / Pa
1.4×10 5
1.0×10 5
2700
70
Residence time / min
70
70
70
130
[0015] The high-molecular-weight polylactic acid melt obtained by polymerization is directly spun, and after initial spinning, one-stage stretching, two-stage stretching, crimping, and finally shaping into filaments, the initial spinning temperature is 245°C, and the speed is 1000-2000m / min. The draw ratio of stretching is 2.5-3.5, the temperature is 120°C, a...
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