Method for preparing cellulose/nanometer titanium dioxide blending material in ionic liquid solvent
A technology of nano-titanium dioxide and ionic liquid solvent, which is applied in the preparation of spinning solution, artificial filament in cellulose solution, wet spinning method, etc., which can solve the lack of adsorption force, difficulty in preparing related materials, interface incompatibility, etc. problems, to avoid pollution, to be beneficial to environmental protection and the health of operators, and to achieve low process energy consumption and operating costs
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Example Embodiment
[0018] Example 1 [BMIM]Cl
[0019] A 50ml three-necked bottle containing 20g of [BMIM]Cl ionic liquid was placed in an oil bath at 100°C. After the temperature was stable, 2g of cotton fiber was added to it, and the addition was divided into six times, 1 time per 5min. The dissolving time of cotton fiber in the ionic liquid was 30 min, then 0.05 g of nano-titanium dioxide was added, and the spinning solution was obtained by stirring for 3 h. After the spinning solution is defoamed, it enters a water coagulation bath through a single-hole spinneret, and the temperature of the coagulation bath is room temperature. After 10% plasticizing and stretching, and then washing, bleaching, drying and other processes, a fiber with a strength of 3.2 cN / dtex and an elongation at break of 18.5% was obtained.
Example Embodiment
[0020] Example 2 [BMIM]BF 4
[0021] Will contain 20g [BMIM]BF 4 A 50ml three-necked bottle of ionic liquid was placed in an oil bath at 80°C. After the temperature was stable, 0.5g of cotton fiber was added to it, and the addition was divided into six times, 1 time / 5min. The dissolving time of cotton fiber in the ionic liquid was 30 min, then 0.01 g of nano-titanium dioxide was added, and the spinning solution was obtained by stirring for 3 h. After the spinning solution is defoamed, it enters a 10% ionic liquid aqueous solution coagulation bath through a single-hole spinneret, and the coagulation bath temperature is room temperature. After 15% plasticizing and stretching, and then washing, bleaching, drying and other processes, a fiber with a strength of 2.7 cN / dtex and an elongation at break of 8.5% is obtained.
Example Embodiment
[0022] Example 3 [BMIM]PF 6
[0023] Will contain 20g [BMIM]PF 6 A 50ml three-necked bottle of ionic liquid was placed in an oil bath at 100°C. After the temperature was stable, 3.5g of cotton fiber was added to it, and the addition was divided into six times, 1 time per 5min. The dissolving time of cotton fiber in the ionic liquid was 30 min, then 0.03 g of nano-titanium dioxide was added, and the spinning solution was obtained by stirring for 3 h. After the spinning solution is defoamed, it enters into a coagulation bath of 20% ionic liquid aqueous solution through a single-hole spinneret, and the coagulation bath temperature is 40°C. After 20% plasticizing and stretching, and then washing, bleaching, drying, etc., a fiber with a strength of 2.3 cN / dtex and an elongation at break of 11.5% is obtained.
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