Vertical type single-component polyurethane waterproof coating and preparation method thereof
A polyurethane waterproof, one-component technology, applied in the direction of polyurea/polyurethane coatings, coatings, etc., can solve problems such as non-curing, and achieve the effects of reducing labor costs, saving labor costs, and convenient construction
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Embodiment 1
[0030] The preparation of vertical single-component polyurethane waterproof coating, in a 500ml ground three-neck bottle equipped with a stirrer, reflux condenser, and thermometer, 15 parts of polyether triol, 6 parts of polyether diol, 25 parts Chlorinated paraffin, 6 parts of talcum powder 1250 mesh, 8 parts of kaolin 800 mesh, 13 parts of heavy calcium, 0.5 part of carbon black, 0.08 part of antioxidant, slowly heat up to 120°C while stirring, vacuum pressure below -0098MPa 2h, lower the temperature below 60°C, add 8 parts of solvent oil, 3 parts of solvent oil, 0.005 parts of defoamer, 0.03 parts of catalyst diisobutyltin dilaurate, 0.01 parts of benzoyl chloride, 4 parts of toluene-2, 4-diisocyanate, the temperature is controlled at 65°C-70°C, under stirring, vacuum dehydration reaction for 2h-3h, after the reaction is completed, the temperature is lowered to below 45°C-55°C, 0.4 parts of MDA solution is added under high-speed stirring, and react After 1 to 2 hours, the t...
Embodiment 2
[0032] For the preparation of vertical one-component polyurethane waterproof coating, 20 parts of polyether trihydric alcohol, 5 parts of polyether glycol, 25 parts of Chlorinated paraffin, 6 parts of talcum powder 1250 mesh, 8 parts of kaolin 800 mesh, 15 parts of heavy calcium, 0.6 part of carbon black, 0.08 part of antioxidant, slowly heat up to 120°C while stirring, vacuum pressure below -0098MPa 2h, lower the temperature below 60°C, add 9 parts of solvent naphtha S150, 2 parts of 200# solvent naphtha, 0.006 parts of defoamer, 0.04 parts of catalyst diisobutyltin dilaurate, 0.01 parts of benzoyl chloride , 3.8 parts of toluene-2,4-diisocyanate, the temperature is controlled at 70 ° C, under stirring, vacuum dehydration reaction for 2h ~ 3h, after the reaction is completed, the temperature is lowered to below 50 ° C, 0.6 parts of MDA solution is added under high-speed stirring, and React for 1 to 2 hours, lower the temperature to below 40°C, and flush the discharge with nit...
Embodiment 3
[0034] For the preparation of vertical one-component polyurethane waterproof coating, in a 500ml ground three-necked bottle equipped with a stirrer, a reflux condenser, and a thermometer, 25 parts of polyether triols, 25 parts of chlorinated paraffin, 7 parts of talcum powder 1250 Mesh, 6 parts of kaolin 800 mesh, 13 parts of heavy calcium, 0.5 parts of carbon black, 0.08 parts of antioxidant, slowly heat up to 120°C under stirring, vacuum pressure below -0098MPa for 2 hours, and lower the temperature to below 60°C , add 9 parts of solvent oil S150, 2 parts of 200# solvent oil, 0.005 parts of defoamer, 0.03 parts of catalyst diisobutyltin dilaurate and mix them, 0.01 parts of benzoyl chloride, 4.5 parts of toluene-2,4- Diisocyanate, the temperature is controlled at 70°C, under stirring, the vacuum dehydration reaction is 2h~3h, after the reaction is completed, the temperature is lowered to below 50°C, and 0.6 parts of MDA solution is added under high-speed stirring, and reacted...
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