Preparation method of semiconductor wafer cutting blade material

A wafer and cutting edge technology, which is applied in the field of semiconductor wafer cutting edge material preparation, can solve the problems of long pickling time, high water consumption, low jet mill output, etc., and achieve good wafer cutting effect, Uniform particle size distribution and good high temperature resistance

Inactive Publication Date: 2010-11-24
HENAN XINDAXIN SCI & TECH
View PDF2 Cites 8 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Since the purity of the silicon material used for semiconductors is generally more than six 9, the price is expensive, so the requirements for the cutting edge are relatively high, and it is difficult to produce such products with ordinary processes
At present, there are mainly the following production methods for cutting blades: the production process of jet mill crushing, the products produced are more than 90% equal in shape, and the yield is also high, but the overall output of jet mill is low, and the produced particles The shape is relatively round, the sharpness is poor, and there are hidden cracks, which are not conducive to cutting; in the prior art, Raymond mills are also used for crushing. Although the output of Raymond mills is high, the yield is low, and the products produced are equal in volume The shape is less, accounting for about 50%, and there are many particles in the shape of needles and flakes, the cutting efficiency is poor, and it is not wear-resistant; in the prior art, there are also traditional wet ball mills for crushing, although the product particles are equal It has many shapes and good sharpness, but the output is low, the yield is low, and the over-grinding is serious; in addition, some existing blade preparation processes still have shortcomings such as long pickling time and high water consumption.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Preparation method of semiconductor wafer cutting blade material
  • Preparation method of semiconductor wafer cutting blade material
  • Preparation method of semiconductor wafer cutting blade material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Embodiment 1 A kind of preparation method of semiconductor wafer cutting edge material, comprises the following steps:

[0033] (1) For raw material crushing, select green silicon carbide block materials with a purity of ≥99% and black silicon carbide block materials to mix according to a mass ratio of 18:1, carry out jaw crushing and sieve, and collect silicon carbide particle size sand with a particle size of ≤3mm;

[0034] (2) Wet ball milling and overflow classification are performed in the wet method frequency conversion ball mill classification device (see figure 1 ) for grinding and grading, add medium balls and silicon carbide particle size sand according to the weight ratio of medium ball: silicon carbide particle size sand of 4:1, the speed of the frequency conversion wet ball mill is 80rpm in the early stage of 0.5h, and the speed of 2h in the middle period is 100rpm. In the later stage 1.5h, the rotation speed is 120rpm, and the water intake is 600L / h; the ...

Embodiment 2

[0043] Embodiment 2 A kind of preparation method of semiconductor wafer cutting edge material, comprises the following steps:

[0044] (1) For raw material crushing, select green silicon carbide block material with a purity of ≥99% and black silicon carbide block material to mix according to a mass ratio of 19:1, carry out jaw crushing and sieve, and collect silicon carbide particle size sand with a particle size of ≤3mm;

[0045] (2) Wet ball milling and overflow classification adopt the same wet method frequency conversion ball mill classification device as in Example 1 for wet milling and classification. When grinding and classifying, the ratio of medium ball: silicon carbide grain size sand is 5:1 The weight ratio of medium balls and silicon carbide particle size sand is added. The speed of the variable frequency wet ball mill is 90rpm in the first 0.6h, 100rpm in the middle 1.9h, 150rpm in the later 1.6h, and the water intake is 500L / h;

[0046] (3) Pickling and vacuum de...

Embodiment 3

[0054] Embodiment 3 A method for preparing a cutting edge of a semiconductor wafer is basically the same as in Embodiment 1, except that in the step (2), the wet grinding is carried out by ordinary wet frequency conversion ball milling, and then the Commonly used hydraulic classifiers are used for classification to obtain silicon carbide powder slurry in the required particle size range.

[0055] The performance indexes of the obtained semiconductor wafer cutting edge material are shown in Table 4.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention relates to a preparation method of a semiconductor wafer cutting blade material. In the preparation method, high-purity green silicon carbide and black silicon carbide are adopted as raw materials, and a wafer cutting blade material is prepared through the steps of jaw crushing and sifting, wet ball milling classification, pickling, overflow size separation, concentrating and dewatering, drying, blending, fine screening and the like. Silicon carbide blade materials prepared through the method are most in equiareal shape and keep sharp edges and strong cutting power, can minimize TTV of a silicon wafer, and have strong adaptability to cutting fluid such as polyethylene glycol and the like because blade material particles have larger specific area and clean surfaces. Products crushed by a wet ball mill are most in equiareal shape, have high output, and can avoid excessive crushing. The preparation method of the invention can reach over 50% of rate of finished products, and products milled with the technology have more uniform size and distribution of particles, thereby better cutting effect to silicon wafers can be achieved.

Description

technical field [0001] The invention relates to the field of multi-wire cutting, in particular to a method for preparing a cutting edge material for a semiconductor wafer. Background technique [0002] With the rapid development of the integrated circuit industry, the demand for high-quality semiconductor wafers is increasing day by day. The processing of semiconductor silicon wafers is an important link in the manufacture of integrated circuits, and effective silicon wafer cutting technology is the basic guarantee for obtaining silicon wafers with high surface accuracy and surface quality. When using the traditional diamond inner circle cutting, with the continuous increase of the wafer diameter, the thickness of the base body of the blade, the thickness of the cutting edge and the difficulty of tensioning the blade increase, the material loss of the kerf and the wear of the blade during cutting increase, and the quality of the silicon wafer decreases. , it is difficult to...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C01B31/36
Inventor 罗小军姜维海宋贺臣郝玉辉李要正
Owner HENAN XINDAXIN SCI & TECH
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products