Method for preparing stain-proof hydrophilic coating from self-crosslinking hydrophilic particles
An antifouling, self-crosslinking technology, used in antifouling/underwater coatings, coatings, biocide-containing paints, etc. To solve the problem of pollution and other problems, to achieve the effect of stable and excellent oil resistance and anti-fouling effect
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Embodiment 1
[0016] (1) Take methoxypolyethylene glycol monomethacrylate (MPEG-MA) with molecular weights of 400, 750, 1000, 1300, and 1500 respectively to carry out the following steps (2) to (7);
[0017] (2) 70 parts by mass of N-methylolacrylamide (N-MAM), 20 parts by mass of methoxypolyethylene glycol monomethacrylate (MPEG-MA), and 10 parts by mass of acrylic acid (AA) were dissolved in In the mixed solvent of 200 mass parts propylene glycol methyl ether (PM) and ethylene glycol butyl ether (EGMA) (the ratio of the mass parts of PM and EGMA is 1: 1), obtain mixed solution I;
[0018] (3) Dissolve 1 mass part of azobisisobutylcyanide (AlBN) in 50 mass parts of propylene glycol monomethyl ether (PM) and ethylene glycol butyl ether (EGMA) (the ratio of mass parts of PM to EGMA is 1:1) In the mixed solvent, the mixed solution II is obtained;
[0019] (4) Mixed solution I and mixed solution II are simultaneously added dropwise to a mixed solvent of 150 parts by mass of propylene glycol m...
Embodiment 2
[0032] (1) Dissolve 70 parts by mass of N-methylolacrylamide (N-MAM), 20 parts by mass of methoxypolyethylene glycol monomethacrylate (MPEG-MA), and 10 parts by mass of acrylic acid (AA) in In the mixed solvent of 200 mass parts propylene glycol methyl ether (PM) and ethylene glycol butyl ether (EGMA) (the ratio of the mass parts of PM and EGMA is 1: 1), obtain mixed solution I;
[0033] (2) Dissolve 1 mass part of azobisisobutylcyanide (AlBN) in 50 mass parts of propylene glycol monomethyl ether (PM) and ethylene glycol butyl ether (EGMA) (the ratio of mass parts of PM to EGMA is 1:1) In the mixed solvent, the mixed solution II is obtained;
[0034] (3) Mixed solution I and mixed solution II are simultaneously added dropwise to a mixed solvent of 150 parts by mass of propylene glycol monomethyl ether (PM) and ethylene glycol butyl ether (EGMA) (the ratio of mass parts of PM to EGMA is 1:1) In the process, the dropwise addition is completed within 4 hours under the condition ...
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