Silicon carbide high-temperature ceramic filter pipe and preparation method thereof
A high-temperature ceramic and silicon carbide technology, which is applied in chemical instruments and methods, filtration separation, separation methods, etc., can solve the problems of limited size and size of porous ceramic products, high energy consumption in the firing process, and poor product uniformity, and achieve thermal stability. Good properties such as permeability and air permeability, high production efficiency, and the effect of reducing the firing time
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Embodiment 1
[0030] The high-temperature silicon carbide ceramic filter tube according to the present invention, its batching weight percentage is composed of: particle diameter is 80-100 micron silicon carbide 72%, high-temperature binder 28%; Additional pore-enhancing agent: charcoal 12%, phenolic resin 2% .
[0031] Among them, the high-temperature binder is composed of 20% talc, 32% refractory clay, 40% potassium feldspar, and 8% alumina, which are mixed for later use.
[0032] Preparation method: mix the aggregate, high-temperature binder, and pore-enhancing agent evenly, age for 24 hours, and pass through a 16-mesh sieve for molding. Put the stale ingredients into the mould, put them into the isostatic press and press to form, the molding pressure is 125MPa, take out the mold after the molding is completed, and get the biscuit after the product is demoulded, and the semi-finished product is obtained after the biscuit is naturally dried. Put the semi-finished product into the kiln ca...
Embodiment 2
[0035] The high-temperature silicon carbide ceramic filter tube of the present invention, its batching weight percentage is composed of: particle diameter is 100-150 micron silicon carbide 75%, high-temperature binder 25%; Additional pore-enhancing agent: charcoal 10%, phenolic resin 1.5% .
[0036] Among them, the high-temperature binder is composed of 23% talc, 35% refractory clay, 30% potassium feldspar, and 12% alumina, which are mixed for later use.
[0037] The production method is that the molding pressure is 100 MPa, the firing temperature is 1330° C., and the holding time is 3 hours. Others are the same as in Example 1, and the obtained product is a silicon carbide ceramic filter tube of φ60×2020 mm.
[0038] Product performance: porosity: 42.2%, average pore diameter: 79 microns, compressive strength: 64.5MPa, thermal shock resistance: 1000°C-20°C cold air 10 times without cracking.
Embodiment 3
[0040] The high-temperature silicon carbide ceramic filter tube according to the present invention, its batching weight percentage is composed of: particle diameter is 200-300 micron silicon carbide 78%, high-temperature binder 22%; Additional pore-enhancing agent: charcoal 8%, phenolic resin 1% .
[0041] Among them, the high-temperature binder ingredients are composed of 22% talc, 32% refractory clay, 35% potassium feldspar, and 11% alumina, which are mixed for later use;
[0042] Preparation method: The molding pressure is 75MPa, the firing temperature is 1370°C, the holding time is 2.2 hours, and the others are the same as in Example 1. The obtained product is a φ60×2000mm silicon carbide ceramic filter tube.
[0043] Product performance: porosity: 48.9%, average pore diameter: 85 microns, thermal shock resistance: 12 times of cold air at 1000°C-20°C without cracking.
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