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Gas-solid/gas-gas phase plasma tubular reactor process and device

A tubular reactor, plasma technology, applied in the direction of plasma, electrical components, chemical/physical/physical-chemical processes of applying energy, etc., can solve the problems of high cost, discontinuous reaction, complex process, etc. Fast, uniform and normal discharge, and the effect of expanding the application field

Inactive Publication Date: 2011-01-05
XINJIANG TIANYE GRP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The purpose of the present invention is to solve the high cost, complex process, environmental pollution and easy bonding and accumulation of solid matter in the reactor when plasma technology is used to meet the special conditions for gas-solid / gas-gas phase reaction in the prior art. Poor quality, discontinuous reaction, instability, etc., and then provide a new reactor that combines tubular reactor and plasma as a reaction catalyst; not only combines the advantages of tubular reactor continuous operation, large production capacity , easy to realize automatic control, realize segmented temperature control, save manpower, large heat transfer area, good mass transfer effect under turbulent flow state, high pressure resistance, simple structure, convenient processing; and the use of plasma has high activity and high reaction speed A Fast Gas-Solid / Gas-Gas Phase Plasma Tubular Reactor Process and Device

Method used

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  • Gas-solid/gas-gas phase plasma tubular reactor process and device

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Embodiment 2

[0023]Embodiment 2 of the present invention is that the hydrogen chloride gas in the reaction gas tank 9 and the nitrogen in the auxiliary gas tank 10 are pressurized with the polyvinyl chloride in the reaction powder equipment 11 after being pressurized by the circulating booster fan 8 whose gas velocity is controlled at 15m / s. The monomers are mixed and sent into the plasma tube reactor 13, chlorine and nitrogen generate low-temperature plasma in the plasma region, and the chlorine-containing gas in the low-temperature plasma state reacts with polyvinyl chloride (PVC), and generates reaction heat at the same time, in order to control the reaction The temperature of the plasma tube reactor 13 is provided with a heat exchange tube 6, and the outer wall of the plasma tube reactor 13 is provided with a tube reactor shell heat exchange insulation layer 7 to ensure that the reactor temperature is controlled at 80 -110°C; the reacted gas and PVC are discharged from the top of the pl...

Embodiment 3

[0024] The difference between embodiment 3 and embodiment 1 or 2 is that the auxiliary gas can be argon or hydrogen.

Embodiment 4

[0025] Embodiment 4 is different from Embodiment 1 or 2 in that: the gas velocity of the blower is 4m / s.

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Abstract

The invention relates to a gas-solid / gas-gas phase plasma tubular reactor process and device, which comprises a circulating booster fan, a reaction gas tank, an auxiliary gas tank, a reaction powder device, a reaction powder intermediate bin, a plasma tubular reactor, a gas-solid separation device, an after-reaction powder intermediate bin, an after-reaction powder conveying device, an after-reaction powder pretreatment device, a product tank and an after-reaction gas treatment device which are communicated in turn. A reaction gas, an auxiliary gas and a solid substance are mixed by the booster fan and then conveyed to the plasma tubular reactor for reaction, the gas phase is recycled by gas-solid separation, and the impurities are discharged and treated; the completely reacted solid phase is conveyed to the product system, and the incompletely reacted solid phase is used for circulating reaction; and the device solves the problems of high cost, complex process and environmental pollution of the conventional process and easy adhesion and accumulation of the solid substance in the reactor, poor product quality, reaction discontinuity and the like in the plasma technology, and can be applied in the chemical chlorination process.

Description

technical field [0001] The invention relates to a gas-solid / gas-gas phase reaction method, in particular to a gas-solid / gas-gas phase plasma tubular reactor process and device. Background technique [0002] With the increasing competitiveness of the chemical industry, many new processes and new reactors have been developed, such as fluidized bed reactors, stirred polycondensation reactors, bioreactors, membrane bioreactors, fixed bed reactors , BASB reactor, industrial C reactor, microwave reactor, ultrasonic reactor, etc., according to different application fields, the development of reactor devices is also becoming more mature and perfect. [0003] In the chemical process, the gas-solid or gas-gas reaction generally completes the reaction process through some specific conditions in the reactor or reactor. This type of reactor has various forms, and many patent documents have also announced it, such as the one published in 01822546.2 Low-cost polyester process using tubula...

Claims

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Application Information

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IPC IPC(8): B01J19/08H05H1/42
Inventor 熊新阳周军郭文康
Owner XINJIANG TIANYE GRP
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