Repairing mass and preparation method thereof

A technology for repairing furnace charge and raw materials, applied in the field of furnace repairing charge and its preparation, can solve the problems of low high temperature flexural strength and adhesion strength, high high temperature strength, short sintering time, etc., so as to shorten the furnace repair time, increase the compressive strength and The effect of anti-scour performance and fast construction speed

Active Publication Date: 2011-02-16
攀枝花钢城集团瑞矿工业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Water-based repairing materials have excellent fluidity and short hardening time, but low high-temperature flexural strength and adhesion strength; non-water-based repairing materials are generally asphalt-bonded, with short sintering time and high high-temperature strength
[0004] The vanadium steelworks where the inventor works, the original vanadium extracting converter repair materials are 75% of mid-grade magnesia, 15% of medium-temperature asphalt, 5% of phenolic resin, 3% of metal aluminum powder, Fe 2 o 3 powder 2%, the sintering time of a single furnace is longer (over 60min), and there are often abnormal damage phenomena such as material collapse, material turning, and rapid erosion, so that the life of a single furnace repair is only about 10 furnaces. Due to the expansion of the production capacity of the vanadium extraction converter, the original repair charge can no longer meet the production needs. Therefore, it is urgent to provide a repair charge with a short sintering time and a long service life to meet the production needs.

Method used

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  • Repairing mass and preparation method thereof
  • Repairing mass and preparation method thereof
  • Repairing mass and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0056] The preparation of embodiment 1 present invention repair charge

[0057] Weigh 55 parts by weight of fused magnesia, 21 parts by weight of sintered magnesia, 15 parts by weight of modified pitch, 2 parts by weight of metal aluminum powder, 2 parts by weight of iron oxide powder, 2.5 parts by weight of caprolactam and 2.5 parts by weight of p-tert-butylphenol , fully mix and stir the weighed fused magnesia, sintered magnesia, modified pitch, metal aluminum powder, iron oxide powder, caprolactam, p-tert-butylphenol, that is, use a mixing mixer to mix and stir, and the mixing time is about for 5min. After the product is formed, it is loaded into a woven bag lined with plastic film from the outlet of the mixer. Simultaneous sampling and detection of chemical composition indicators (see Table 3 for index detection)

Embodiment 2

[0058] Embodiment 2 The preparation of the present invention's mending charge

[0059] Weigh 55 parts by weight of fused magnesia, 22 parts by weight of sintered magnesia, 14 parts by weight of modified pitch, 2 parts by weight of metal aluminum powder, 2 parts by weight of iron oxide powder, 2.5 parts by weight of caprolactam, and 2.5 parts by weight of p-tert-butylphenol , fully mix and stir the weighed fused magnesia, sintered magnesia, modified pitch, metal aluminum powder, iron oxide powder, caprolactam, p-tert-butylphenol, that is, use a mixing mixer to mix and stir, and the mixing time is about for 5min. After the product is formed, it is loaded into a woven bag lined with plastic film from the outlet of the mixer. Simultaneous sampling and detection of chemical composition indicators (see Table 3 for index detection)

Embodiment 3

[0060] Embodiment 3 The preparation of the present invention repair charge

[0061] Weigh 55 parts by weight of fused magnesia, 23 parts by weight of sintered magnesia, 13 parts by weight of modified pitch, 2 parts by weight of metal aluminum powder, 2 parts by weight of iron oxide powder, 2.5 parts by weight of caprolactam, and 2.5 parts by weight of p-tert-butylphenol , fully mix and stir the weighed fused magnesia, sintered magnesia, modified pitch, metal aluminum powder, iron oxide powder, caprolactam, p-tert-butylphenol, that is, use a mixing mixer to mix and stir, and the mixing time is about for 5min. After the product is formed, it is loaded into a woven bag lined with plastic film from the outlet of the mixer. Simultaneous sampling and detection of chemical composition indicators (see Table 4 for index detection)

[0062] Table 4 physical and chemical index detection

[0063]

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Abstract

The invention relates to a repairing mass for repairing in the converter production process of steel making and vanadium extracting of steel enterprises, in particular to a repairing mass used for a converter lining made of magnesia carbon bricks and a preparation method thereof, and provides a repairing mass having the advantages of short sintering time and long service life for meeting the requirement of production. The repairing mass per 100 weight parts comprises the following raw materials in parts by weight: 48-60 parts of fused magnesia, 22-28 parts of magnesite clinker, 10-16 parts ofmodified asphalt, 1-5 parts of metallic aluminum powder, 1-4 parts of ferric oxide powder and 2-10 parts of adhesive. The preparation method of the repairing mass is simple and convenient, i.e. all the raw materials are mixed. In the fettling production process of the vanadium extracting converter, when a local breakage appears on the converter lining, the repairing mass is coated on the part to be repaired; the repairing mass is sintered by utilizing the wall temperature of the converter, and production by blending with iron can be carried out after sintering; and under the conditions of lowsmelting temperature (1,360-1,400 DEG C) of the vanadium extracting converter and shorter smelting period (5-10 minutes), the repairing mass still can be quickly sintered with a working lining to form an organic combination with higher strength so as to prolong the service life of the repairing mass.

Description

technical field [0001] The invention relates to a repair charge used in repairing a vanadium-extracting converter for steelmaking in iron and steel enterprises, in particular to a repair charge used for turning the lining of a vanadium-extracting converter into a magnesia-carbon brick and a preparation method thereof. Background technique [0002] Most of the steelmaking in large iron and steel enterprises is marked by converter steelmaking. Furnace age is one of the important indicators of steelmaking level. Among them, vanadium extraction converter production is a relatively special smelting process. The vanadium slag is extracted through the converter vanadium extraction process to reach efficient use of resources. Due to the particularity of the vanadium extraction process of the converter, the lining material of the converter is not only chemically corroded by high-temperature molten steel and slag during use, but also mechanically scoured by molten iron and scrap steel...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/66
Inventor 陈涛吴斌吴胜利黄国炳郑德明毛朋
Owner 攀枝花钢城集团瑞矿工业有限公司
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