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Method for refining separated or dispersion-strengthening type block copper alloy crystal particles

A technology of dispersion strengthening and copper alloy, which is applied in the field of bulk ultra-fine-grained high-strength and high-conductivity copper alloy, fine precipitation or dispersion-strengthened bulk copper alloy grains, which can solve the problems of reduced ductility, difficulty in large-scale production, and limitations and other problems, to achieve the effect of convenient operation, simple equipment requirements, saving mold and thermal processing costs

Inactive Publication Date: 2012-04-25
CENT SOUTH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The preparation of bulk ultra-fine-grained high-strength and high-conductivity copper alloys must solve the problems of existing technologies that limit the size of materials such as shape and length, difficulty in large-scale production, and sharp decline in ductility

Method used

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  • Method for refining separated or dispersion-strengthening type block copper alloy crystal particles
  • Method for refining separated or dispersion-strengthening type block copper alloy crystal particles
  • Method for refining separated or dispersion-strengthening type block copper alloy crystal particles

Examples

Experimental program
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Effect test

Embodiment 1

[0029] Cut the high-strength and high-conductivity beryllium-bronze alloy hot-rolled plate into rectangular blocks, place it in the furnace, heat it to 800°C for 60 minutes, then water quench and cool it, then place the sample on the lower flat anvil of the hydraulic press, and compress it with the X-axis first. The shaft undergoes compression deformation. When the true strain in the X direction reaches 0.2, stop the compression, rotate the sample 90 degrees, take the Y axis as the compression axis, and compress again. When the true strain in the Y direction reaches 0.2, stop the compression and rotate the sample 90 degrees degrees, take the Z axis as the compression axis, and compress again. When the true strain in the Z direction reaches 0.2, the compression is stopped, the sample is rotated 90 degrees, and then the X axis is used as the compression axis, and the compression in the X→Y→Z→X direction is repeated. Anneal at 800°C when the true strain in each direction reaches...

Embodiment 2

[0031] Place the high-strength and high-conductivity beryllium-bronze alloy rectangular hot forging block in the furnace, heat it to 820°C for 40 minutes, then water quench and cool it, then place the sample on the lower flat anvil of the hydraulic press, and first perform compression deformation with the X-axis as the compression axis . When the true strain in the X direction reaches 0.3, the compression is stopped, and the sample is rotated 90 degrees, with the Y axis as the compression axis, and compressed again. When the true strain in the Y direction reaches 0.3, the compression is stopped, and the sample is rotated 90 degrees, with the Z axis as the compression axis, and compressed again. When the true strain in the Z direction reaches 0.3, the compression is stopped, the sample is rotated 90 degrees, and then the X axis is used as the compression axis, and the compression in the X→Y→Z→X direction is repeated. When the cumulative true strain in each direction reaches 2....

Embodiment 3

[0033] Cut the high-strength and high-conductivity beryllium-bronze alloy hot-rolled plate into rectangular blocks, place it in a furnace, heat it to 850°C for 120 minutes, then water quench and cool it, then place the sample on the lower flat anvil of the hydraulic press, and compress it with the X-axis first. The shaft undergoes compression deformation. When the true strain in the X direction reaches 0.4, the compression is stopped, and the sample is rotated 90 degrees, with the Y axis as the compression axis, and compressed again. When the true strain in the Y direction reaches 0.4, the compression is stopped, and the sample is rotated 90 degrees, with the Z axis as the compression axis, and compressed again. When the true strain in the Z direction reaches 0.4, the compression is stopped, the sample is rotated 90 degrees, and the X-axis is used as the compression axis, and the compression in the X→Y→Z→X direction is repeated. When the true strain in each direction accumula...

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Abstract

The invention relates to a method for coordinating and refining high-strength and high conductivity copper alloy crystal particles by using room temperature multidirection deformation and annealing process, which comprises the following steps of cutting high-strength and high conductivity copper alloy ingot or thermal deformation section into rectangular blocks, putting the blocks in a furnace, heating to 800 to 860 DEG C, preserving the heat for 40 to 120 hours, quenching with water, cooling and carrying out multi-round and multi-axis compression deformation in sequence along an X axis, a Y axis and a Z axis of the rectangular blocks, and controlling the true dependent variable of each round to be 0.2 to 0.6, annealing and recrystallizing at 600 to 800 DEG C when the accumulated true dependent variable is more than 1.2 so that superfine crystal particle copper alloy blocks of which the mean size is 0.5 to 3 mum are obtained. The method has simple requirements on processing technique and equipment, is convenient for operation, and is capable of effectively overcoming the defects of serious damage of moulds, too high requirements on power and difficult preparation of block materials in the process of refining the high-strength and high conductivity copper alloy crystal particles in the prior art; in addition, the method can be used for preparing a large dense superfine crystal particle copper alloy material and has good industrial application prospect.

Description

technical field [0001] The invention discloses a method for refining precipitated or dispersion-strengthened bulk copper alloy grains, in particular to use room temperature multi-directional deformation and annealing to coordinate refine copper alloy grains and prepare bulk ultrafine grain high-strength and high-conductivity copper alloy. The invention belongs to the technical field of copper alloy processing. Background technique [0002] Precipitation-strengthened or dispersion-strengthened high-strength and high-conductivity copper alloy is a high-performance functional material with excellent electrical conductivity, thermal conductivity and non-ferromagnetism. It is also a structural material with high strength and toughness and can withstand large loads. It has important application value and broad application prospects in the fields of transportation, electrical and electronics. [0003] Grain refinement is a commonly used strengthening method for metals. From the ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22F1/08
Inventor 杨续跃蔡小华张雷
Owner CENT SOUTH UNIV