Quality control method of children lung clearing pills serving as Chinese medicinal preparation
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A quality control method and technology of traditional Chinese medicine preparations, applied in the direction of medical formula, drug combination, measuring device, etc., can solve the problem of no quality control method for Xiaoer Qingfei Pills
Active Publication Date: 2011-05-11
津药达仁堂集团股份有限公司达仁堂制药厂
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Although there is no international standard for botanical Chinese medicines in the world at present, the United States, the European Union, my country, and Southeast Asia, where traditional Chinese medicines are traditionally exported, all have a tendency to raise the standards of Chinese medicines. Standards, my country has a history of thousands of years of traditional Chinese medicine use, countries around the world refer to our coun
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[0047] Below in conjunction with the examples, the present invention is further described, the following examples are illustrative, not limiting, and the protection scope of the present invention cannot be limited by the following examples.
[0048] The quality control method of Chinese medicine preparation Xiaoer Qingfei Pills, the steps of the method are:
[0049] (1) Microscopic identification:
[0050] Observe under a microscope: the fiber bundles are pale yellow, and the surrounding parenchyma cells contain square crystals of calcium oxalate to form crystal fibers (licorice). Pollen grains are spherical, about 22-33 μm in diameter, with spines on the outer wall, about 3 μm long, with 3 germination holes (inplex flowers). Bast fiber light yellow, fusiform, thick wall, fine pores and grooves (Scutellaria baicalensis). Palisade cells of testa are yellow-brown, polygonal in surface view, thick in wall, tightly arranged (radish seeds). The cells of the endocarp tissue fragm...
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Abstract
The invention relates to a quality control method of children lung clearing pills serving as a Chinese medicinal preparation. The method comprises the steps of: firstly, performing microscopical identification; secondly, identifying whether a prescription of the children lung clearing pills comprises platycodon root, pummelo peel, bitter orange, whiteflower hogfennel root and white mulberry root-bark or not by a thin layer chromatography; and lastly, detecting the baical skullcap root content of the prescription of the children lung clearing pills by taking baicalin as a comparison substance by a liquid chromatography. The quality standard of the children lung clearing pills is enhanced and perfected; based on the original standard, a microscopical identification method is provided for liquoric root, inula flower, baical skullcap root, radish seed and perilla fruit; a thin-layer identification method for whiteflower hogfennel root, white mulberry root-bark, platycodon root, bitter orange and pummelo peel in the prescription is drawn up; and a content test method for the baical skullcap root in the prescription is set up by taking baicalin as a comparison substance. By a modified quality standard, the quality control method of a product is enhanced, and counterfeit medicaments and substandard medicaments can be inspected more correctly; and the standard plays an important role in the modernization and overseas development of traditional Chinese medicines.
Description
technical field [0001] The invention belongs to the technical field of traditional Chinese medicines, and relates to a detection method of traditional Chinese medicines, in particular to a quality control method of Xiaoer Qingfei Pills, a traditional Chinese medicine preparation. Background technique [0002] Xiaoer Qingfei Pills are composed of Peucedanum Peucedanum, Trichosanthes Fen, Mint, Morus alba, Bitter Almond (stir-fried), Perilla Seed, Campanulaceae, Perilla, Licorice, Inulae Inulae, Fructus Citrus Fructus Citrus Fructus, Radix Fructus Radix, Radix Scutellariae, Fuhai Stone (calcined) composition, the above fifteen flavors, crushed into fine powder, sieved, and mixed. Add 110-130g of refined honey to every 100g of powder to make big honeyed pills. Functions and indications are clearing the lung and relieving the exterior, relieving cough and reducing phlegm, used for acute bronchitis, wind-heat cold, cough, spit white sticky phlegm or yellow thick phlegm. [0003...
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