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Method for preparing carbon nano tube electrode

A carbon nanotube and electrode technology, applied in the field of carbon nanotube electrode preparation, can solve the problems of limited removal ability of PPCPs and so on

Inactive Publication Date: 2011-06-01
BEIJING UNIV OF CHEM TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0007] The effluent discharge of sewage treatment plants is considered to be a very important way. At present, general urban sewage treatment plants are designed and constructed to remove organic matter and some nutrients, and their ability to remove PPCPs is limited.

Method used

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  • Method for preparing carbon nano tube electrode

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Embodiment

[0026] Example: Electrolysis of triclosan with a palladium-coated carbon nanotube electrode.

[0027] First prepare a certain concentration of triclosan solution (in which the supporting electrolyte is sodium sulfate, the concentration is 1000mg / L), after adjusting the pH with NaOH and sulfuric acid, add it to the electrolytic cell, start the magnetic stirrer, set the electrolysis voltage to 30V, and Start the electrolysis at the next step, and after 10 hours of electrolysis, the removal rate of triclosan reaches more than 95%, and the dechlorination rate reaches 85%.

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Abstract

The invention discloses a method for preparing a carbon nano tube electrode used for persistent organic matter electrolysis. The carbon nano tube arouses worldwide research interest owning to unique mechanical and electronic properties as well as chemical stability, the carbon nano tube can effectively promote electronic transmission of biological matters and environmental substances, and researchers pay an increasing attention to the relation between the electrochemical activity mechanism of the carbon nano tube and the morphological structure, the preparation method and the surface modification of the carbon nano tube in recent years. The carbon nano tube electrode is prepared by utilizing the advantages of the carbon nano tube, and different modifications are carried out on the carbon nano tube, thus the carbon nano tube can be applied to the degradation of different pollutants. The carbon nano tube electrode is prepared by regulating the ratio of the carbon nano tube to polytetrafluoroethylene to metal used for modification, the prepared electrode has the advantages of simple preparation process, high strength, long service life, good conductivity and the like, and the dechlorination rate can reach more than 85% after reaction occurs for a period of time when the electrode is applied to electrochemical degradation of triclosan-containing solution.

Description

technical field [0001] The invention relates to a method for preparing a carbon nanotube electrode. The electrode has a simple preparation process and stable performance. After modification, it can be used for electrolyzing persistent organic pollutants, especially some chlorinated organic substances, and is an excellent electrode. Background technique [0002] In 1991, Japanese scientist Iijima used a high-resolution electron microscope to study vacuum arc-evaporated graphite, and discovered a multi-layered tube of carbon with nanometer dimensions, that is, multi-walled carbon nanotubes. This discovery has attracted extensive attention from the physics, chemistry, material science and high-tech industry departments, and has set off another research climax after C60. The unique physical and chemical properties of carbon nanotubes, such as extremely high mechanical strength, good adsorption capacity and strong microwave absorption energy, are increasingly recognized by people...

Claims

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Application Information

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IPC IPC(8): C02F1/461
Inventor 胡翔叶文彬
Owner BEIJING UNIV OF CHEM TECH
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