Modified chopped fiber of permanent porous high-moisture-absorption quick-drying terylene and preparation method thereof
A polyester modified, microporous technology, applied in the field of spinning, can solve the problems of increasing the cost of filaments, application limitations, difficulty, damage, etc., and achieve the effect of good softness
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Embodiment 1
[0057] 1. A method for producing polyester modified slices with a preliminary microporous structure tendency, comprising the following steps:
[0058] 1) At first, purified terephthalic acid, ethylene glycol, polyethylene glycol, dimethyl isophthalate-5-sodium sulfonate and ethylene glycol antimony and triphenyl phosphate are mixed in proportioning by weight Sufficient mixing and slurrying in the slurry tank;
[0059] 2) Next, the mixed slurry is introduced into an esterification kettle for esterification reaction, and the esterification temperature is controlled at 258°C;
[0060] 3) again, in the polycondensation still, Polyethylene Glycol and dimethyl isophthalate-5-sodium sulfonate and esterification reaction gained oligomer bishydroxyethyl terephthalate carry out reaction polycondensation and obtain a kind of Polyester modified stock solution slurry with pore structure tendency, in which the polycondensation reaction temperature is 292°C, and the vacuum degree is 72Pa; ...
Embodiment 2
[0110] 1. A method for producing polyester modified slices with a preliminary microporous structure tendency, comprising the following steps:
[0111] 1) At first, purified terephthalic acid, ethylene glycol, polyethylene glycol, dimethyl isophthalate-5-sodium sulfonate and ethylene glycol antimony and triphenyl phosphate are mixed in proportioning by weight Sufficient mixing and slurrying in the slurry tank;
[0112] 2) Next, the slurry is introduced into an esterification kettle for esterification reaction, and the esterification temperature is controlled at 200°C;
[0113] 3) again, in the polycondensation still, Polyethylene Glycol and dimethyl isophthalate-5-sodium sulfonate and esterification reaction gained oligomer bishydroxyethyl terephthalate carry out reaction polycondensation and obtain a kind of Polyester modified stock solution slurry with pore structure trend, in which the polycondensation reaction temperature is 245°C, and the vacuum degree is 80Pa;
[0114] ...
Embodiment 3
[0162] 1. A method for producing polyester modified slices with a preliminary microporous structure tendency, comprising the following steps:
[0163] 1) At first, purified terephthalic acid, ethylene glycol, polyethylene glycol, dimethyl isophthalate-5-sodium sulfonate and ethylene glycol antimony and triphenyl phosphate are mixed in proportioning by weight Sufficient mixing and slurrying in the slurry tank;
[0164] 2) Next, the slurry is introduced into an esterification kettle for esterification reaction, and the esterification temperature is controlled at 280°C;
[0165] 3) again, in the polycondensation still, polyoxyethylene glycol and dimethyl isophthalate-5-sodium sulfonate and the oligomer bishydroxyethyl terephthalate of esterification gained carry out reaction polycondensation and obtain a kind of having Polyester modified stock solution slurry with microporous structure trend, wherein the polycondensation reaction temperature is 300°C, and the vacuum degree is 30...
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