Production process of aluminium sulfate by using aluminum ores

A production process, aluminum ore technology, applied in the field of inorganic chemical material manufacturing, can solve the problems of long construction period, high price, high product cost, etc., and achieve the effect of saving manpower and material resources, shortening the production cycle and improving production efficiency

Inactive Publication Date: 2011-08-10
周广强
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The prior art scheme has the following defects: when producing liquid aluminum sulfate, the settling time of the solid-liquid mixture discharged from the reactor in the settling tank is generally 1 to 2 days before a part of the aluminum sulfate solution can be obtained; It still contains a large amount of aluminum sulfate, which must be washed again or even multiple times to obtain the remaining aluminum sulfate. Therefore, the construction period is long and the production efficiency is low, resulting in huge product costs and high prices; when producing solid aluminum sulfate, it is also because The liquid aluminum sulfate used contains a lot of water and is at normal temperature. During the evaporation process, a lot of heat energy is needed, so the production cost is further increased.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] A production process for preparing liquid aluminum sulfate from aluminum ore, the steps are: crush the aluminum ore with a pulverizer, transport it to a storage bin, and screen it with a 50-60 mesh sieve; The purpose is to add the aluminum ore powder into the water-filled mixer, and mix the aluminum ore powder and water in the ratio of 1:1 to 0.8 by mass percentage, fully stir and mix them, and transport them to the reaction kettle; add 93 to 98% concentrated Sulfuric acid into the reaction kettle, wherein the mass percentage of the above-mentioned pasty aluminum ore powder and concentrated sulfuric acid is 1:1; the above-mentioned mixture is stirred to make it undergo a sufficient chemical reaction for 2 to 3 hours; at this time, the The temperature is 145~155℃, and the pressure is 0.25~0.27MPa;

[0041]Discharge the solid-liquid mixture in the reaction kettle into a dilution tank filled with an appropriate amount of water, dilute and cool down, so that the density of ...

Embodiment 2

[0043] A production process for preparing solid aluminum sulfate from aluminum ore. The steps are: crush the aluminum ore with a crusher, transport it to a storage bin, and use a 50-60 mesh sieve to screen it; The purpose is to add the aluminum ore powder into the water-filled mixer, and mix the aluminum ore powder and water in the ratio of 1:1 to 0.8 by mass percentage, fully stir and mix them, and transport them to the reaction kettle; add 93 to 98% concentrated Put sulfuric acid into the reaction kettle, wherein the mass percentage of the above-mentioned pasty aluminum ore powder and concentrated sulfuric acid is 1:1; stir the above-mentioned mixture to make it undergo a sufficient chemical reaction for 2 to 3 hours; at this time, the reaction kettle The temperature is 145~155℃, and the pressure is 0.25~0.27MPa;

[0044] Drain the solid-liquid mixture in the reaction kettle into the dilution insulation tank, add a small amount of water to dilute and cool down, and keep the ...

Embodiment 3

[0047] A production process for preparing solid aluminum sulfate from aluminum ore. The steps are: crush the aluminum ore with a crusher, transport it to a storage bin, and use a 50-60 mesh sieve to screen it; The purpose is to add the aluminum ore powder into the water-filled mixer, and mix the aluminum ore powder and water in the ratio of 1:1 to 0.8 by mass percentage, fully stir and mix them, and transport them to the reaction kettle; add 93 to 98% concentrated Put sulfuric acid into the reaction kettle, wherein the mass percentage of the above-mentioned pasty aluminum ore powder and concentrated sulfuric acid is 1:1; stir the above-mentioned mixture to make it undergo a sufficient chemical reaction for 2 to 3 hours; at this time, the reaction kettle The temperature is 145~155℃, and the pressure is 0.25~0.27MPa;

[0048] The solid-liquid mixture in the reactor is transported to the insulated two-way centrifugal pump through the insulated pipeline, and then the solid-liquid ...

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Abstract

The invention discloses a production process of aluminium sulfate by using aluminum ores. The method comprises the following steps: a) adding aluminum ore powder paste and concentrated sulfuric acid in a reaction kettle to perform a chemical reaction; b) discharging the obtained solid-liquid mixture to a thinning tank to dilute and cool; c) conveying the solid-liquid mixture in a filter press to perform filter pressing and obtain an aluminium sulfate solution; d) performing acid-base neutralization on the aluminium sulfate solution to obtain a liquid aluminium sulfate product; e) heating the aluminium sulfate solution to evaporate; and f) delivering the evaporated aluminium sulfate solution to a crystallizing steel band, and performing air blowing and water cooling to obtain solid aluminium sulfate. The method has the following advantages: the existing sedimentation method is not adopted, and the solid-liquid mixture is subjected to filter pressing to obtain the liquid aluminium sulfate product, the product has low moisture so that a lot of heat energy can be saved during evaporation and the cost can be reduced; the production time is half an hour, thus the production cycle can be shortened, labor can be saved and the efficiency can be high; the filter pressing of the solid-liquid mixture can be directly performed to obtain an aluminium sulfate solution; and the aluminium sulfate solution is not evaporated and is directly delivered to the crystallizing steel band to prepare the solid aluminium sulfate through air blowing and water cooling.

Description

technical field [0001] The invention belongs to the technical field of manufacturing inorganic chemical materials, and in particular relates to a production process for preparing aluminum sulfate from aluminum ore. Background technique [0002] As an inorganic salt product, aluminum sulfate is widely used in industry. It is mainly used as a sizing agent in the paper industry, a flocculant in drinking water purification, industrial water purification, and industrial wastewater treatment. It can also be used in purification Fats and oils, pharmaceutical cosmetics, fire extinguishing agents, leather tanning and the production of various compound aluminum salts, etc. The main components of aluminum ore include alumina and silica. The use of aluminum ore to prepare aluminum sulfate is mainly due to the reaction of alumina and sulfuric acid to produce aluminum sulfate. At present, most of its production processes are as follows: crush aluminum ore into particles, put it in a reac...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01F7/74
Inventor 周广强
Owner 周广强
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