Ageing-resistant road asphalt based on magnesium-aluminum-based laminar double hydroxide and preparation method thereof
A technology of double hydroxide and road asphalt, which is used in building structures, building components, building thermal insulation materials, etc., can solve the problems that the anti-aging agent asphalt is difficult to play, the asphalt becomes hard and brittle, and the performance of asphalt pavement is damaged. , to achieve excellent UV blocking effect, achieve long-term effectiveness, and improve the effect of aging resistance
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Embodiment 1
[0018] 2 parts (parts by mass, the same below) of magnesium-aluminum-based layered double hydroxide (formed as Mg 0.75 al 0.25 (OH) 2 (CO 3 ) 0.12 1.2H 2 O, and surface-modified by petroleum sulfonate, the particle size in the a and b directions is 2.1 μm, and the grain thickness in the c-axis direction is 0.13 μm, about 110 layers) After adding 98 parts, the temperature has risen to 140 °C In the asphalt (softening point 48°C, penetration 82dmm), keep the temperature at 140-150°C and stir at 4000rpm for 1.5h to obtain a magnesium-aluminum-based layered double hydroxide aging-resistant road asphalt.
[0019] The magnesium-aluminum-based layered double hydroxide aging-resistant road asphalt was subjected to an ultraviolet aging test (the irradiation intensity of the ultraviolet lamp was 1200 μW / cm 2 , irradiated for 6 days, the same below), the viscosity at 135°C before and after aging increased from 850cp to 1570cp, an increase of 720cp, and the ductility at 5°C decreased...
Embodiment 2
[0021] Add 5 parts of magnesium-aluminum-based layered double hydroxide to 95 parts of asphalt (softening point 48°C, penetration 82dmm) that has been heated to 150°C, keep the temperature at 150-160°C, and stir at 3000rpm for 2h , to obtain a magnesium-aluminum-based layered double hydroxide aging-resistant road asphalt.
[0022] The viscosity at 135°C of the magnesium-aluminum-based layered double hydroxide aging-resistant road asphalt before and after ultraviolet aging increased from 930cp to 1420cp, an increase of 788cp, and the softening point increased from 49.1°C to 53.2°C, an increase of 4.1°C. For ordinary road asphalt without magnesium-aluminum-based layered double hydroxide, the viscosity at 135°C increased from 620cp to 2100cp before and after ultraviolet aging, an increase of 1480cp, and the softening point increased from 48°C to 56.3°C, an increase of 8.5°C. Similar to Example 1, the aging-resistant road asphalt added with magnesium-aluminum-based layered double ...
Embodiment 3
[0024]Add 8 parts of magnesium-aluminum-based layered double hydroxide to 92 parts of asphalt (softening point 48°C, penetration 82dmm) that has been heated to 150°C, keep the temperature at 150-160°C, and stir at 6000rpm for 2h , to obtain a magnesium-aluminum-based layered double hydroxide aging-resistant road asphalt.
[0025] The viscosity at 135°C of the magnesium-aluminum-based double hydroxide aging-resistant road asphalt before and after ultraviolet aging increased from 1100cp to 1310cp, an increase of 210cp, and the ductility at 5°C decreased from 9.5cm to 6.2cm, a decrease of 3.3cm. For ordinary road asphalt without magnesium-aluminum-based layered double hydroxide, the viscosity at 135°C increased from 620cp to 2100cp before and after ultraviolet aging, an increase of 1480cp, and the ductility at 5°C decreased from 10.5cm to 3.4cm, a decrease of 7.1cm. Similar to Example 1, the aging-resistant road asphalt added with magnesium-aluminum-based layered double hydroxide...
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