Corrosion inhibitor for controlling corrosion of high-concentration hydrogen sulfide in acid liquor medium and preparation method thereof
A corrosion inhibitor and high-concentration technology, applied in earthwork drilling, organic chemistry, wellbore/well components, etc., can solve the problems of unsatisfactory hydrogen stress corrosion effects, achieve excellent corrosion inhibition performance, enhance adsorption capacity, combine good effect
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Embodiment 1
[0043] The first step: Synthesis of 2-amino-5-methylthiazole:
[0044] Add 73.6g of n-propanol and 3.2g of water into a 250mL three-necked bottle equipped with a thermometer, stirrer, air guide tube, tail gas tube and an alkali absorption bottle, weigh and record. At 10°C (if necessary, cool with water or ice water), slowly introduce chlorine gas, and start the stirrer to stir. When the weight of the three-necked bottle reaches 24.5g-49g, stop the chlorine gas flow. The cumulative time for chlorine gas injection is From 2h to 4h, the amount of chlorine gas introduced is 1 / 3mol. Separate the heavy layer, add 10.5 g of a mixture of thiourea and water with a weight ratio of 2.5:1, heat up to 60-90°C and heat to reflux, and simultaneously use copper sulfate test solution or thin-layer chromatography to detect the reaction. The reaction time is about 4 After ~5h, propanol was recovered by distillation, and an oily substance was obtained in the three-necked flask. Add 2.1 g of wat...
Embodiment 2
[0051] The first step: Synthesis of 2-amino-5-methylthiazole:
[0052] Add 73.6g of n-propanol and 3.2g of water into a 250mL three-necked bottle equipped with a thermometer, stirrer, air guide tube, tail gas tube and an alkali absorption bottle, weigh and record. At 10°C (if necessary, cool with water or ice water), slowly introduce chlorine gas, and start the stirrer to stir. When the weight of the three-necked bottle reaches 24.5g-49g, stop the chlorine gas flow. The cumulative time for chlorine gas injection is From 2h to 4h, the amount of chlorine gas introduced is 1 / 3mol. Separate the heavy layer, add 10.5 g of a mixture of thiourea and water with a weight ratio of 2.5:1, heat up to 60-90°C and heat to reflux, and simultaneously use copper sulfate test solution or thin-layer chromatography to detect the reaction. The reaction time is about 4 After ~5h, propanol was recovered by distillation, and an oily substance was obtained in the three-necked flask. Add 2.1 g of wat...
Embodiment 3
[0058] The first step: Synthesis of 2-amino-5-methylthiazole:
[0059] Add 73.6g of n-propanol and 3.2g of water into a 250mL three-necked bottle equipped with a thermometer, stirrer, air guide tube, tail gas tube and an alkali absorption bottle, weigh and record. At 10°C (if necessary, cool with water or ice water), slowly introduce chlorine gas, and start the stirrer to stir. When the weight of the three-necked bottle reaches 24.5g-49g, stop the chlorine gas flow. The cumulative time for chlorine gas injection is From 2h to 4h, the amount of chlorine gas introduced is 1 / 3mol. Separate the heavy layer, add 10.5 g of a mixture of thiourea and water with a weight ratio of 2.5:1, heat up to 60-90°C and heat to reflux, and simultaneously use copper sulfate test solution or thin-layer chromatography to detect the reaction. The reaction time is about 4 After ~5h, propanol was recovered by distillation, and an oily substance was obtained in the three-necked flask. Add 2.1 g of wat...
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