Dielectric ceramic and laminated ceramic capacitor
A technology for dielectric ceramics and capacitors, which is applied in multilayer capacitors, capacitors, fixed capacitors, etc., can solve the problems of high-temperature load life characteristics that are not clear, and the dielectric ceramic layer is not described, and achieves the effect of excellent life characteristics.
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experiment example 1
[0036] (A) Production of Dielectric Ceramic Raw Materials
[0037] As a starting material, prepare BaCO as microparticles 3 , CaCO 3 and TiO 2 of each powder. Then, these powders are used to become the main component (Ba 1-x / 100 Ca x / 100 ) 1.01 TiO 3 After weighing according to the method of the composition, they were mixed using a ball mill. Here, the Ca amount x is as shown in the "Ca amount x" column of Table 1.
[0038] Next, the above-mentioned mixed powder was synthesized by calcining to obtain (Ba 1-x / 100 Ca x / 100 ) 1.01 TiO 3Main ingredient powder. The average particle diameter of the obtained main component powder was about 10 nm. In addition, when using XRD, the unreacted substances in the main component powder were below the detection level. That is, it was confirmed that the main component powder is a powder with a high degree of synthesis although it is a very small particle.
[0039] On the other hand, prepare MgO and MnCO as subcomponents 3 , SiO...
experiment example 2
[0070] In Experimental Example 2, the influence of impurities was evaluated.
[0071] In the manufacturing process of laminated ceramic capacitors such as raw material production, Sr, Zr, Hf, Zn, Na, Ag, Pd, and Ni may be mixed into dielectric ceramics as impurities, and they may exist in crystal particles and occupy In the crystal grain boundary between crystal grains. In addition, during the firing process of multilayer ceramic capacitors, etc., internal electrode components may diffuse and exist in the crystal grains in the dielectric ceramic and occupy the crystal grain boundaries between the crystal grains. In Experimental Example 2, the influence of these impurities was evaluated.
[0072] (A) Production of Dielectric Ceramic Raw Materials
[0073] In the composition formula: 100(Ba 0.95 Ca 0.05 )TiO 3 +2.0MgO+1.8SiO 2 +1.0MnO+8.0DyO 3 / 2 Except for adding the impurity components shown in Table 3 to the shown composition, a dielectric ceramic raw material was obtai...
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